1,6-BIS(DICHLOROMETHYLSILYL)HEXANE

Base Information

• Chemical Name: 1,6-BIS(DICHLOROMETHYLSILYL)HEXANE
• CAS No.: 18395-97-6
• Molecular Formula: C₈H₁₈Cl₄Si₂
• Molecular Weight: 312.214
• Hs Code.: 2931900090
• Mol file: 18395-97-6.mol

Synonyms:2,9-Disiladecane,2,2,9,9-tetrachloro- (6CI,8CI); Silane, 1,6-hexanediylbis[dichloromethyl-(9CI); 1,6-Bis(dichloromethylsilyl)hexane

Chemical Property of 1,6-BIS(DICHLOROMETHYLSILYL)HEXANE

Chemical Property:

• Boiling Point: 119 °C
• PSA: 0.00000
• Density: 1,131 g/cm3
• LogP: 5.64600

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Statements: 34
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,6-BIS(DICHLOROMETHYLSILYL)HEXANE

There total 4 articles about 1,6-BIS(DICHLOROMETHYLSILYL)HEXANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dichloromethylsilane (75-54-7) + 1,5-Hexadien (592-42-7) → Si,Si,Si',Si'-tetrachloro-Si,Si'-dimethyl-Si,Si'-hexanediyl-bis-silane (18395-97-6)

Guidance literature:

tetrakis(triphenylphosphine)platinum; at 45 - 52 ℃;

DOI:10.1002/hlca.19710540510

Reference yield:

1,5-Hexadien (592-42-7) + dimethylsilicon dichloride (75-78-5,30107-43-8) → Si,Si,Si',Si'-tetrachloro-Si,Si'-dimethyl-Si,Si'-hexanediyl-bis-silane (18395-97-6)

Guidance literature:

With dihydrogen hexachloroplatinate; In isopropyl alcohol; Heating;

DOI:10.1246/bcsj.37.871

Reference yield:

Dichloromethylsilane (75-54-7) + 1,5-Hexadien (592-42-7) → Si,Si,Si',Si'-tetrachloro-Si,Si'-dimethyl-Si,Si'-hexanediyl-bis-silane (18395-97-6) + C7H14Cl2Si + 5-hexenylmethyldichlorosilane (90054-19-6) + trans-1-(Methyl-dichlor-silyl)-hexen-4 (33602-94-7)

Guidance literature:

With hydrogen hexachloroplatinate(IV) monohydrate; In isopropyl alcohol; at 20 ℃; for 24h;

DOI:10.1080/10426500701693388

upstream raw materials:

Dichloromethylsilane

1,5-Hexadien

dimethylsilicon dichloride

Downstream raw materials:

1,6-bis(trimethylsilyl)hexane