(S)-((2R,3S)-3-((tert-butyldiphenylsilyloxy)methyl)-2-methyloxiran-2-yl)((2R,3R)-2,3-dimethyloxiran-2-yl)methanol

Base Information

Chemical Name:(S)-((2R,3S)-3-((tert-butyldiphenylsilyloxy)methyl)-2-methyloxiran-2-yl)((2R,3R)-2,3-dimethyloxiran-2-yl)methanol
CAS No.:1192305-77-3
Molecular Formula:C₂₅H₃₄O₄Si
Molecular Weight:426.628
Hs Code.:

Synonyms:(S)-((2R,3S)-3-((tert-butyldiphenylsilyloxy)methyl)-2-methyloxiran-2-yl)((2R,3R)-2,3-dimethyloxiran-2-yl)methanol

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Chemical Property of (S)-((2R,3S)-3-((tert-butyldiphenylsilyloxy)methyl)-2-methyloxiran-2-yl)((2R,3R)-2,3-dimethyloxiran-2-yl)methanol

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Technology Process of (S)-((2R,3S)-3-((tert-butyldiphenylsilyloxy)methyl)-2-methyloxiran-2-yl)((2R,3R)-2,3-dimethyloxiran-2-yl)methanol

There total 1 articles about (S)-((2R,3S)-3-((tert-butyldiphenylsilyloxy)methyl)-2-methyloxiran-2-yl)((2R,3R)-2,3-dimethyloxiran-2-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1192305-76-2
(S,2Z,5E)-1-(tert-butyldiphenylsilyloxy)-3,5-dimethylhepta-2,5-dien-4-ol

: 1192305-77-3
(S)-((2R,3S)-3-((tert-butyldiphenylsilyloxy)methyl)-2-methyloxiran-2-yl)((2R,3R)-2,3-dimethyloxiran-2-yl)methanol

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 4 ℃; Inert atmosphere;
DOI:10.1021/ol901853t

Reference yield: 71.0%

: 1192305-77-3
(S)-((2R,3S)-3-((tert-butyldiphenylsilyloxy)methyl)-2-methyloxiran-2-yl)((2R,3R)-2,3-dimethyloxiran-2-yl)methanol

: 100-39-0
benzyl bromide

: 1192305-78-4
(((2S,3S)-3-((S)-benzyloxy((2S,3R)-2,3-dimethyloxiran-2-yl)methyl)-3-methyloxiran-2-yl)methoxy)(tert-butyl)diphenylsilane

Guidance literature:: (S)-((2R,3S)-3-((tert-butyldiphenylsilyloxy)methyl)-2-methyloxiran-2-yl)((2R,3R)-2,3-dimethyloxiran-2-yl)methanol; With sodium hydride; In tetrahydrofuran; at 65 - 70 ℃; Inert atmosphere;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; at 65 - 70 ℃; for 3h;
DOI:10.1021/ol901853t