4-methoxycarbonyl-3-nitrophenyl isothiocyanate

Base Information

• Chemical Name: 4-methoxycarbonyl-3-nitrophenyl isothiocyanate
• CAS No.: 808123-16-2
• Molecular Formula: C₉H₆N₂O₄S
• Molecular Weight: 238.224
• Mol file: 808123-16-2.mol

Synonyms:4-methoxycarbonyl-3-nitrophenyl isothiocyanate

Chemical Property of 4-methoxycarbonyl-3-nitrophenyl isothiocyanate

Chemical Property:

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Technology Process of 4-methoxycarbonyl-3-nitrophenyl isothiocyanate

There total 1 articles about 4-methoxycarbonyl-3-nitrophenyl isothiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

methyl-2-nitro-4-amino-benzoate (84228-45-5) + 1,1'-Thiocarbonyldi-2(1H)-pyridone (102368-13-8) → 4-methoxycarbonyl-3-nitrophenyl isothiocyanate (808123-16-2)

Guidance literature:

In dichloromethane; at 20 ℃; for 3h;

Reference yield: 85.0%

4-methoxycarbonyl-3-nitrophenyl isothiocyanate (808123-16-2) → methyl 4-hydrazinocarbonothioylamino-2-nitrobenzoate

Guidance literature:

With methylhydrazine; In tetrahydrofuran; at 0 ℃; for 1h;

upstream raw materials:

methyl-2-nitro-4-amino-benzoate

1,1'-Thiocarbonyldi-2(1H)-pyridone