2-(2-Benzenesulfinyl-ethyl)-2-(benzhydrylidene-amino)-5-oxo-hexanoic acid ethyl ester

Base Information

Chemical Name:2-(2-Benzenesulfinyl-ethyl)-2-(benzhydrylidene-amino)-5-oxo-hexanoic acid ethyl ester
CAS No.:137283-05-7
Molecular Formula:C₂₉H₃₁NO₄S
Molecular Weight:489.635
Hs Code.:

Synonyms:2-(2-Benzenesulfinyl-ethyl)-2-(benzhydrylidene-amino)-5-oxo-hexanoic acid ethyl ester

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Chemical Property of 2-(2-Benzenesulfinyl-ethyl)-2-(benzhydrylidene-amino)-5-oxo-hexanoic acid ethyl ester

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Technology Process of 2-(2-Benzenesulfinyl-ethyl)-2-(benzhydrylidene-amino)-5-oxo-hexanoic acid ethyl ester

There total 3 articles about 2-(2-Benzenesulfinyl-ethyl)-2-(benzhydrylidene-amino)-5-oxo-hexanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 137283-22-8
4-Benzenesulfinyl-2-(benzhydrylidene-amino)-butyric acid ethyl ester

: 78-94-4,25038-87-3
methyl vinyl ketone

: 137283-05-7
2-(2-Benzenesulfinyl-ethyl)-2-(benzhydrylidene-amino)-5-oxo-hexanoic acid ethyl ester

Guidance literature:: With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; at 60 ℃; for 1h;
DOI:10.1080/00397919108021572

Reference yield:

: 69555-14-2
ethyl N-diphenylmethylene glycine

: 137283-05-7
2-(2-Benzenesulfinyl-ethyl)-2-(benzhydrylidene-amino)-5-oxo-hexanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / K₂CO₃, benzyltriethylammonium chloride (TEBACl) / 1 h / 60 °C

2: 91 percent / K₂CO₃, benzyltriethylammonium chloride (TEBACl) / 1 h / 60 °C

With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate;
DOI:10.1080/00397919108021572

Reference yield:

: 20451-53-0
Phenyl vinyl sulfoxide

: 137283-05-7
2-(2-Benzenesulfinyl-ethyl)-2-(benzhydrylidene-amino)-5-oxo-hexanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / K₂CO₃, benzyltriethylammonium chloride (TEBACl) / 1 h / 60 °C

2: 91 percent / K₂CO₃, benzyltriethylammonium chloride (TEBACl) / 1 h / 60 °C

With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate;
DOI:10.1080/00397919108021572