2-[2-methyl-2-(4-methylphenylsulfonyl)-1-oxopropyl]-9H-thioxanthen-9-one 10-oxide

Base Information

• Chemical Name: 2-[2-methyl-2-(4-methylphenylsulfonyl)-1-oxopropyl]-9H-thioxanthen-9-one 10-oxide
• CAS No.: 1040390-25-7
• Molecular Formula: C₂₄H₂₀O₅S₂
• Molecular Weight: 452.552
• Mol file: 1040390-25-7.mol

Synonyms:2-[2-methyl-2-(4-methylphenylsulfonyl)-1-oxopropyl]-9H-thioxanthen-9-one 10-oxide

Chemical Property of 2-[2-methyl-2-(4-methylphenylsulfonyl)-1-oxopropyl]-9H-thioxanthen-9-one 10-oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[2-methyl-2-(4-methylphenylsulfonyl)-1-oxopropyl]-9H-thioxanthen-9-one 10-oxide

There total 1 articles about 2-[2-methyl-2-(4-methylphenylsulfonyl)-1-oxopropyl]-9H-thioxanthen-9-one 10-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-(2-bromo-2-methyl-1-oxopropyl)-9H-thioxanthen-9-one 10-oxide (1040390-24-6) + sodium 4-methylbenzenesulfinate (824-79-3) → 2-[2-methyl-2-(4-methylphenylsulfonyl)-1-oxopropyl]-9H-thioxanthen-9-one 10-oxide (1040390-25-7)

Guidance literature:

In dimethyl sulfoxide; at 20 - 25 ℃; for 0.5h;

DOI:10.1134/S1070428009010230

Reference yield: 47.0%

n-phenoxyheptane (32395-96-3) + 2-[2-methyl-2-(4-methylphenylsulfonyl)-1-oxopropyl]-9H-thioxanthen-9-one 10-oxide (1040390-25-7) → 10-(4-heptyloxyphenyl)-2-[2-methyl-2-(4-methylphenylsulfonyl)-1-oxopropyl]thioxanthen-10-ium hexafluorophosphate(V)

Guidance literature:

n-phenoxyheptane; 2-[2-methyl-2-(4-methylphenylsulfonyl)-1-oxopropyl]-9H-thioxanthen-9-one 10-oxide; With methanesulfonic acid; phosphorus pentoxide; at 20 - 25 ℃; for 3.5h;

With potassium hexafluorophosphate; In water; at 5 ℃; for 0.5h;

DOI:10.1134/S1070428009010230

upstream raw materials:

2-(2-bromo-2-methyl-1-oxopropyl)-9H-thioxanthen-9-one 10-oxide

sodium 4-methylbenzenesulfinate