C₅₉H₈₄O₁₂

Base Information

Chemical Name:C₅₉H₈₄O₁₂
CAS No.:676549-21-6
Molecular Formula:C₅₉H₈₄O₁₂
Molecular Weight:985.309
Hs Code.:

C<sub>59</sub>H<sub>84</sub>O<sub>12</sub>

Synonyms:C₅₉H₈₄O₁₂

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Chemical Property of C₅₉H₈₄O₁₂

Chemical Property:

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Technology Process of C₅₉H₈₄O₁₂

There total 25 articles about C₅₉H₈₄O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 197899-19-7
(2R)-1-chloro-2-hydroxy-4-pentene

: 676549-21-6
C₅₉H₈₄O₁₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: 81 percent / KOH

2.1: n-BuLi / tetrahydrofuran / -78 - 20 °C

2.2: BF₃*Et₂O / tetrahydrofuran / 0.33 h / -78 °C

2.3: 75 percent / tetrahydrofuran / 1 h / -78 °C

3.1: 77 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 20 °C

4.1: NaH / dimethylformamide / 0.17 h

4.2: 73 percent / Bu₄NI / dimethylformamide / 25 h / 20 °C

5.1: n-BuLi / tetrahydrofuran / 0.17 h / -50 °C

5.2: 434 mg / tetrahydrofuran / 0.5 h / -40 °C

6.1: 32 percent / (S,S)-salen Co(III)OAc; H₂O / tetrahydrofuran / 1 h

7.1: n-BuLi / tetrahydrofuran; hexane / 2.5 h / -78 - -40 °C

7.2: Bf₃*Et₂O / tetrahydrofuran; hexane / 0.17 h / -78 °C

7.3: 59 percent / tetrahydrofuran; hexane / 3 h / -78 °C

8.1: 100 °C

9.1: Pt(DVDS) / tetrahydrofuran; xylene / 20 °C

10.1: aq. H₂O₂; KF; KHCO₃ / tetrahydrofuran; methanol / 20 °C

11.1: Et₂BOMe / tetrahydrofuran; methanol / -78 °C

11.2: NaBH₄ / tetrahydrofuran; methanol / -78 °C

12.1: K₂CO₃; MeOH

13.1: TsOH*H₂O; 3 Angstroem molecular sieves / 20 °C

With methanol; potassium fluoride; potassium hydroxide; n-butyllithium; bis(η2:η2-1,3-divinyltetramethyl)platinum(0); (S,S)-salen Co(III)OAc; 3 A molecular sieve; diethyl methoxy borane; water; dihydrogen peroxide; sodium hydride; potassium carbonate; potassium hydrogencarbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; xylene;
DOI:10.1021/ja039618+

Reference yield:

: 144422-60-6
(R)-2-but-3-enyloxirane

: 676549-21-6
C₅₉H₈₄O₁₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: n-BuLi / tetrahydrofuran / -78 - 20 °C

1.2: BF₃*Et₂O / tetrahydrofuran / 0.33 h / -78 °C

1.3: 75 percent / tetrahydrofuran / 1 h / -78 °C

2.1: 77 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 20 °C

3.1: NaH / dimethylformamide / 0.17 h

3.2: 73 percent / Bu₄NI / dimethylformamide / 25 h / 20 °C

4.1: n-BuLi / tetrahydrofuran / 0.17 h / -50 °C

4.2: 434 mg / tetrahydrofuran / 0.5 h / -40 °C

5.1: 32 percent / (S,S)-salen Co(III)OAc; H₂O / tetrahydrofuran / 1 h

6.1: n-BuLi / tetrahydrofuran; hexane / 2.5 h / -78 - -40 °C

6.2: Bf₃*Et₂O / tetrahydrofuran; hexane / 0.17 h / -78 °C

6.3: 59 percent / tetrahydrofuran; hexane / 3 h / -78 °C

7.1: 100 °C

8.1: Pt(DVDS) / tetrahydrofuran; xylene / 20 °C

9.1: aq. H₂O₂; KF; KHCO₃ / tetrahydrofuran; methanol / 20 °C

10.1: Et₂BOMe / tetrahydrofuran; methanol / -78 °C

10.2: NaBH₄ / tetrahydrofuran; methanol / -78 °C

11.1: K₂CO₃; MeOH

12.1: TsOH*H₂O; 3 Angstroem molecular sieves / 20 °C

With methanol; potassium fluoride; n-butyllithium; bis(η2:η2-1,3-divinyltetramethyl)platinum(0); (S,S)-salen Co(III)OAc; 3 A molecular sieve; diethyl methoxy borane; water; dihydrogen peroxide; sodium hydride; potassium carbonate; potassium hydrogencarbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; xylene;
DOI:10.1021/ja039618+

Reference yield:

: 323192-62-7
(4S,5S)-4,6-dimethyl-5-(p-methoxybenzyloxy)-trans-hept-2-enal

: 676549-21-6
C₅₉H₈₄O₁₂

Guidance literature:: Multi-step reaction with 15 steps

1.1: K₂CO₃; MeOH / 3 h / 20 °C

2.1: 2.22 g / TsOH*H₂O; 3 Angstroem molecular sieves / 17 h / 20 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 2.5 h / -60 - -40 °C

3.2: BF₃*Et₂O / tetrahydrofuran; hexane / 0.25 h / -78 °C

3.3: 82 percent / tetrahydrofuran; hexane / 1.5 h / -78 °C

4.1: 15 h / 100 °C

5.1: Pt(DVDS) / tetrahydrofuran; xylene / 21 h / 20 °C

6.1: 545 mg / TsOH*H₂O; 3 Angstroem molecular sieves / 21 h / 20 °C

7.1: n-BuLi / tetrahydrofuran; hexane / 2.5 h / -78 - -40 °C

7.2: Bf₃*Et₂O / tetrahydrofuran; hexane / 0.17 h / -78 °C

7.3: 59 percent / tetrahydrofuran; hexane / 3 h / -78 °C

8.1: 100 °C

9.1: Pt(DVDS) / tetrahydrofuran; xylene / 20 °C

10.1: aq. H₂O₂; KF; KHCO₃ / tetrahydrofuran; methanol / 20 °C

11.1: Et₂BOMe / tetrahydrofuran; methanol / -78 °C

11.2: NaBH₄ / tetrahydrofuran; methanol / -78 °C

12.1: K₂CO₃; MeOH

13.1: TsOH*H₂O; 3 Angstroem molecular sieves / 20 °C

With methanol; potassium fluoride; n-butyllithium; bis(η2:η2-1,3-divinyltetramethyl)platinum(0); 3 A molecular sieve; diethyl methoxy borane; dihydrogen peroxide; potassium carbonate; potassium hydrogencarbonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; hexane; xylene;
DOI:10.1021/ja039618+