Bis(triphenylmethyl)trisulfane

Base Information

• Chemical Name: Bis(triphenylmethyl)trisulfane
• CAS No.: 58451-52-8
• Molecular Formula: C₃₈H₃₀S₃
• Molecular Weight: 582.854

Synonyms:Bis(triphenylmethyl)trisulfane

Chemical Property of Bis(triphenylmethyl)trisulfane

Chemical Property:

Purity/Quality:

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Technology Process of Bis(triphenylmethyl)trisulfane

There total 6 articles about Bis(triphenylmethyl)trisulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

n-butyllithium (109-72-8,29786-93-4) + α,α-diphenylbenzenemethanesulfenyl chloride (35572-83-9) → ditrityl disulfide (15446-31-8) + Bis(triphenylmethyl)trisulfane (58451-52-8) + Butyl(triphenylmethyl)disulfane

Guidance literature:

In diethyl ether; at -78 ℃;

DOI:10.1021/jo00083a022

Reference yield: 38.0%

tritylsulfenyl chloride (24165-03-5) → Bis(triphenylmethyl)trisulfane (58451-52-8)

Guidance literature:

With sodium hydrogensulfide; In diethyl ether; for 24h; Ambient temperature;

DOI:10.1021/jo00083a022

Reference yield:

α,α-diphenylbenzenemethanesulfenyl chloride (35572-83-9) → ditrityl disulfide (15446-31-8) + Bis(triphenylmethyl)trisulfane (58451-52-8) + Butyl(triphenylmethyl)disulfane

Guidance literature:

With n-butyllithium; In diethyl ether; at -78 ℃; Yields of byproduct given;

DOI:10.1021/jo00083a022

upstream raw materials:

n-butyllithium

α,α-diphenylbenzenemethanesulfenyl chloride

tritylsulfenyl chloride

triphenylmethanedithiosulfenyl chloride

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