1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethylamine triflouroacetate

Base Information

Chemical Name:1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethylamine triflouroacetate
CAS No.:1100767-60-9
Molecular Formula:C₂HF₃O₂*C₁₂H₁₆F₃NO₂
Molecular Weight:377.284
Hs Code.:

Synonyms:1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethylamine triflouroacetate

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Chemical Property of 1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethylamine triflouroacetate

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Technology Process of 1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethylamine triflouroacetate

There total 2 articles about 1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethylamine triflouroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1100767-58-5
1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethanone

: 76-05-1
trifluoroacetic acid

: 1100767-60-9
1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethylamine triflouroacetate

Guidance literature:: 1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethanone; With ammonium acetate; In methanol; at 20 ℃; for 3h;

With sodium cyanoborohydride; In methanol; for 6h; Heating / reflux;

trifluoroacetic acid;

Reference yield:

: 208173-24-4
1-(4-fluoro-3-(trifluoromethyl)phenyl)ethanone

: 1100767-60-9
1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethylamine triflouroacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / dimethyl sulfoxide / 1 h / 20 °C

1.2: 1 h

2.1: ammonium acetate / methanol / 3 h / 20 °C

2.2: 6 h / Heating / reflux

With ammonium acetate; sodium hydride; In methanol; dimethyl sulfoxide;

Reference yield: 25.0%

: 1100767-60-9
1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethylamine triflouroacetate

: 1100767-27-8
N-(4-carbamimidoyl-phenyl)-malonamic acid trifluoroacetate

: 1100767-61-0
N-(4-carbamimidoyl-phenyl)-N'-{1-[4-(2-methoxy-ethoxy)-3-trifluoromethyl-phenyl]-ethyl}-malonamide

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 24h;