5-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2-methoxyphenyl chloroacetate

Base Information

Chemical Name:5-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2-methoxyphenyl chloroacetate
CAS No.:1344112-11-3
Molecular Formula:C₂₁H₂₁ClO₉
Molecular Weight:452.845
Hs Code.:

Synonyms:5-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2-methoxyphenyl chloroacetate

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Chemical Property of 5-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2-methoxyphenyl chloroacetate

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Technology Process of 5-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2-methoxyphenyl chloroacetate

There total 2 articles about 5-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2-methoxyphenyl chloroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 18780-67-1
4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoic acid

: 30287-15-1
2-methoxyphenyl 2-chloroacetate

: 1344112-11-3
5-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2-methoxyphenyl chloroacetate

Guidance literature:: With eaton’s reagent; at 60 ℃;
DOI:10.1016/j.bioorg.2020.103643

Reference yield:

: 90-05-1
2-methoxy-phenol

: 1344112-11-3
5-{4-[(ethoxycarbonyl)oxy]-3,5-dimethoxybenzoyl}-2-methoxyphenyl chloroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 8 h / 135 °C / Inert atmosphere

2: methanesulfonic acid; phosphorus pentoxide / 3 h / 50 °C / Inert atmosphere

With methanesulfonic acid; phosphorus pentoxide; 2: Friedel Crafts acylation;
DOI:10.1016/j.bmc.2011.08.047