4-methyl-N'-(1,4-dioxaspiro[4.5]decan-8-ylidene)benzenesulfonohydrazide

Base Information

Chemical Name:4-methyl-N'-(1,4-dioxaspiro[4.5]decan-8-ylidene)benzenesulfonohydrazide
CAS No.:195436-65-8
Molecular Formula:C₁₅H₂₀N₂O₄S
Molecular Weight:324.401
Hs Code.:

Synonyms:4-methyl-N'-(1,4-dioxaspiro[4.5]decan-8-ylidene)benzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-N'-(1,4-dioxaspiro[4.5]decan-8-ylidene)benzenesulfonohydrazide

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Technology Process of 4-methyl-N'-(1,4-dioxaspiro[4.5]decan-8-ylidene)benzenesulfonohydrazide

There total 1 articles about 4-methyl-N'-(1,4-dioxaspiro[4.5]decan-8-ylidene)benzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 4746-97-8
cyclohexanedione monoethylene ketal

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 195436-65-8
4-methyl-N'-(1,4-dioxaspiro[4.5]decan-8-ylidene)benzenesulfonohydrazide

Guidance literature:: In 1,4-dioxane; at 130 ℃; for 1h; Microwave irradiation;
DOI:10.1016/j.bmcl.2014.10.060

Reference yield: 77.0%

: 6783-05-7
trans-2-phenylvinylboronic acid

: 195436-65-8
4-methyl-N'-(1,4-dioxaspiro[4.5]decan-8-ylidene)benzenesulfonohydrazide

: 8-(2-phenylethylidene)-1,4-dioxaspiro[4.5]decane

Guidance literature:: With potassium carbonate; cesium fluoride; In 1,4-dioxane; at 150 ℃; for 0.5h; regioselective reaction; Microwave irradiation;
DOI:10.1002/anie.201200683

Reference yield: 49.0%

: 15022-93-2,40389-50-2
Z-α-bromostilbene

: 195436-65-8
4-methyl-N'-(1,4-dioxaspiro[4.5]decan-8-ylidene)benzenesulfonohydrazide

: (E)-8-(1,2-diphenylvinyl)-1,4-dioxaspiro[4.5]dec-7-ene

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; lithium tert-butoxide; XPhos; In 1,4-dioxane; at 130 ℃; for 12h; Inert atmosphere;
DOI:10.1002/adsc.201601155