C₄₁H₅₆O₄

Base Information

Chemical Name:C₄₁H₅₆O₄
CAS No.:1246949-31-4
Molecular Formula:C₄₁H₅₆O₄
Molecular Weight:612.893
Hs Code.:

C<sub>41</sub>H<sub>56</sub>O<sub>4</sub>

Synonyms:C₄₁H₅₆O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₅₆O₄

Chemical Property:

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Technology Process of C₄₁H₅₆O₄

There total 13 articles about C₄₁H₅₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1266102-56-0
C₄₁H₅₄O₅

: 1246949-31-4
C₄₁H₅₆O₄

Guidance literature:: With hydrazine hydrate; potassium hydroxide; In ethylene glycol; Inert atmosphere;
DOI:10.1021/jo102054r

Reference yield: 85.0%

: 107297-16-5
C₂₇H₄₄O₄

: 100-39-0
benzyl bromide

: 1246949-31-4
C₄₁H₅₆O₄

Guidance literature:: C₂₇H₄₄O₄; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 1h; Inert atmosphere;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; mineral oil; at 0 ℃; Inert atmosphere; Reflux;
DOI:10.1021/ol1019663

Reference yield:

: 1246949-44-9
3-OTBS-11-ketotigogenin

: 1246949-31-4
C₄₁H₅₆O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran / -10 °C / Inert atmosphere; Reflux

4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

4.2: 0 °C / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; sodium hydride; triphenylphosphine; In tetrahydrofuran; mineral oil; 2.1: Mitsunobu reaction;
DOI:10.1021/jo102054r