N-<(-ethylthio)acetyl>-N-(4-hydroxybenzyl)-N'-(3-diazopyruvoyl)-1,3-phenylenediamine

Base Information

Chemical Name:N-<(-ethylthio)acetyl>-N-(4-hydroxybenzyl)-N'-(3-diazopyruvoyl)-1,3-phenylenediamine
CAS No.:160777-03-7
Molecular Formula:C₂₀H₂₀N₄O₄S
Molecular Weight:412.469
Hs Code.:

Synonyms:N-<(-ethylthio)acetyl>-N-(4-hydroxybenzyl)-N'-(3-diazopyruvoyl)-1,3-phenylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<(-ethylthio)acetyl>-N-(4-hydroxybenzyl)-N'-(3-diazopyruvoyl)-1,3-phenylenediamine

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Technology Process of N-<(-ethylthio)acetyl>-N-(4-hydroxybenzyl)-N'-(3-diazopyruvoyl)-1,3-phenylenediamine

There total 6 articles about N-<(-ethylthio)acetyl>-N-(4-hydroxybenzyl)-N'-(3-diazopyruvoyl)-1,3-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 160777-00-4
N-bromoacetyl-N-(4-hydroxybenzyl)-N'-(3-diazopyruvoyl)-1,3-phenylenediamine

: 75-08-1
ethanethiol

: 160777-03-7
N-<(-ethylthio)acetyl>-N-(4-hydroxybenzyl)-N'-(3-diazopyruvoyl)-1,3-phenylenediamine

Guidance literature:: With N-methylenemorpholine; In water; acetone; for 15h;
DOI:10.1021/jo00126a055

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 160777-03-7
N-<(-ethylthio)acetyl>-N-(4-hydroxybenzyl)-N'-(3-diazopyruvoyl)-1,3-phenylenediamine

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / ethanol / 18 h

2: 98 percent / sodium cyanoborohydride, ZnCl₂ / methanol / 3 h

3: 77 percent / N-methylenemorpholine / ethyl acetate / 1 h / 0 °C

4: 79 percent / N-methylenemorpholine / acetone; H₂O / 15 h

With N-methylenemorpholine; sodium cyanoborohydride; zinc(II) chloride; In methanol; ethanol; water; ethyl acetate; acetone;
DOI:10.1021/jo00126a055

Reference yield:

: 108-45-2,64554-26-3,76583-20-5
m-phenylenediamine

: 160777-03-7
N-<(-ethylthio)acetyl>-N-(4-hydroxybenzyl)-N'-(3-diazopyruvoyl)-1,3-phenylenediamine

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / ethyl acetate / 12 h

2: 76 percent / ethanol / 18 h

3: 98 percent / sodium cyanoborohydride, ZnCl₂ / methanol / 3 h

4: 77 percent / N-methylenemorpholine / ethyl acetate / 1 h / 0 °C

5: 79 percent / N-methylenemorpholine / acetone; H₂O / 15 h

With N-methylenemorpholine; sodium cyanoborohydride; zinc(II) chloride; In methanol; ethanol; water; ethyl acetate; acetone;
DOI:10.1021/jo00126a055