7,9-Bis-O-(2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone

Base Information

Chemical Name:7,9-Bis-O-(2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone
CAS No.:132817-52-8
Molecular Formula:C₅₂H₄₆F₆N₄O₂₁
Molecular Weight:1176.94
Hs Code.:

Synonyms:7,9-Bis-O-(2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone

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Chemical Property of 7,9-Bis-O-(2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone

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Technology Process of 7,9-Bis-O-(2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone

There total 2 articles about 7,9-Bis-O-(2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.3%

: 76050-95-8,95626-27-0,103301-86-6,103301-89-9,21288-60-8,132677-57-7
ε-Rhodomycinone

: 132814-67-6
1-O-tert-butyldimethylsilyl 4-O-p-nitrobenzoyl-2,3,6-trideoxy-3-trifluoroacetamido-β-L-lyxo-hexopyranoside

: 132817-52-8
7,9-Bis-O-(2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone

: 132817-51-7,132882-05-4
7-O-(2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; acetone; at -35 ℃; for 16h;
DOI:10.1016/0008-6215(91)80147-F

Reference yield: 32.0%

: 76050-95-8,95626-27-0,103301-86-6,103301-89-9,21288-60-8,132677-57-7
ε-Rhodomycinone

: 132817-48-2
2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-1-O-trimethylsilyl-α-L-lyxo-hexopyranose

: 132817-52-8
7,9-Bis-O-(2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone

: 132817-53-9
2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

: 132817-51-7,132882-05-4
7-O-(2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone

: 132817-51-7,132882-05-4
7-O-(2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-β-L-lyxo-hexopyranosyl)-ε-rhodomycinone

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at -35 ℃; Further byproducts given;
DOI:10.1016/0008-6215(91)80147-F