2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-1-O-trimethylsilyl-α-L-lyxo-hexopyranose

Base Information

Chemical Name:2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-1-O-trimethylsilyl-α-L-lyxo-hexopyranose
CAS No.:132817-48-2
Molecular Formula:C₁₈H₂₃F₃N₂O₇Si
Molecular Weight:464.471
Hs Code.:

Synonyms:2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-1-O-trimethylsilyl-α-L-lyxo-hexopyranose

Suppliers and Price of 2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-1-O-trimethylsilyl-α-L-lyxo-hexopyranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-1-O-trimethylsilyl-α-L-lyxo-hexopyranose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-1-O-trimethylsilyl-α-L-lyxo-hexopyranose

There total 2 articles about 2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-1-O-trimethylsilyl-α-L-lyxo-hexopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.3%

: 75-77-4
chloro-trimethyl-silane

: 76753-25-8,76753-31-6,76753-32-7,76760-23-1,81312-34-7,81312-35-8
2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-L-lyxo-hexopyranose

: 132817-48-2
2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-1-O-trimethylsilyl-α-L-lyxo-hexopyranose

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 12h;
DOI:10.1016/0008-6215(91)80147-F

Reference yield:

: 81312-33-6
Methyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

: 132817-48-2
2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-1-O-trimethylsilyl-α-L-lyxo-hexopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent aq. trifluoroacetic acid / 0.17 h / Heating

2: 93.3 percent / pyridine / CH₂Cl₂ / 12 h / 0 °C

With pyridine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/0008-6215(91)80147-F

Reference yield: 32.0%

: 76050-95-8,95626-27-0,103301-86-6,103301-89-9,21288-60-8,132677-57-7
ε-Rhodomycinone

: 132817-48-2
2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-1-O-trimethylsilyl-α-L-lyxo-hexopyranose

: 132817-52-8
7,9-Bis-O-(2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone

: 132817-53-9
2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl 2,3,6-trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranoside

: 132817-51-7,132882-05-4
7-O-(2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-α-L-lyxo-hexopyranosyl)-ε-rhodomycinone

: 132817-51-7,132882-05-4
7-O-(2,3,6-Trideoxy-4-O-p-nitrobenzoyl-3-trifluoroacetamido-β-L-lyxo-hexopyranosyl)-ε-rhodomycinone

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at -35 ℃; Further byproducts given;
DOI:10.1016/0008-6215(91)80147-F