N-(Diphenylphosphinyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(Diphenylphosphinyl)-4-methylbenzenesulfonamide
CAS No.:6002-24-0
Molecular Formula:C₁₉H₁₈NO₃PS
Molecular Weight:371.397
Hs Code.:
DSSTox Substance ID:DTXSID601231630
Nikkaji Number:J3.381.256F

Synonyms:N-(Diphenylphosphinyl)-4-methylbenzenesulfonamide;DTXSID601231630;6002-24-0

Suppliers and Price of N-(Diphenylphosphinyl)-4-methylbenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(Diphenylphosphinyl)-4-methylbenzenesulfonamide

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:371.07450161
Heavy Atom Count:25
Complexity:544

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NP(=O)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of N-(Diphenylphosphinyl)-4-methylbenzenesulfonamide

There total 5 articles about N-(Diphenylphosphinyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 5994-87-6
diphenylphosphinamide

: 98-59-9
p-toluenesulfonyl chloride

: 6002-24-0
N-(diphenylphosphoryl)-4-methylbenzenesulfonamide

Guidance literature:: diphenylphosphinamide; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

p-toluenesulfonyl chloride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2019.06.013

Reference yield: 26.0%

: 941-55-9
4-toluenesulfonyl azide

: 2071-21-8
bis(diphenylphosphoryl)methane

: 6002-24-0
N-(diphenylphosphoryl)-4-methylbenzenesulfonamide

: 17391-60-5
Diazomethylenbis(diphenylphosphanoxid)

Guidance literature:: With hydrogenchloride; potassium tert-butylate; Yield given. Multistep reaction; 1) benzene, THF, 30 min., reflux; 2) 2 h, room temp.;

Reference yield: 9.0%

: 2071-21-8
bis(diphenylphosphoryl)methane

: 6002-24-0
N-(diphenylphosphoryl)-4-methylbenzenesulfonamide

: 17391-60-5
Diazomethylenbis(diphenylphosphanoxid)

Guidance literature:: With 4-toluenesulfonyl azide; potassium tert-butylate; Yield given. Multistep reaction; 1) benzene, THF, 30 min., reflux; 2) 2 h, room temp.;