cyclohexyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3-methyl-1-oxobutyl)amino-β-D-glucopyranoside

Base Information

Chemical Name:cyclohexyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3-methyl-1-oxobutyl)amino-β-D-glucopyranoside
CAS No.:79284-60-9
Molecular Formula:C₂₃H₃₇NO₉
Molecular Weight:471.548
Hs Code.:

Synonyms:cyclohexyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3-methyl-1-oxobutyl)amino-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclohexyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3-methyl-1-oxobutyl)amino-β-D-glucopyranoside

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Technology Process of cyclohexyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3-methyl-1-oxobutyl)amino-β-D-glucopyranoside

There total 1 articles about cyclohexyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3-methyl-1-oxobutyl)amino-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 79284-59-6
C₁₇H₂₆BrNO₈

: 108-93-0
cyclohexanol

: 79284-60-9
cyclohexyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3-methyl-1-oxobutyl)amino-β-D-glucopyranoside

Guidance literature:: In benzene; for 120h;
DOI:10.1016/S0040-4020(01)97937-2

Reference yield: 46.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 79284-60-9
cyclohexyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3-methyl-1-oxobutyl)amino-β-D-glucopyranoside

: 79284-61-0
cyclohexyl 4,6-O-benzylidene-2-deoxy-2-(3-methyl-1-oxobutyl)amino-β-D-glucopyranoside

Guidance literature:: toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 40 ℃; for 2h;
DOI:10.1016/S0040-4020(01)97937-2

Reference yield:

: 79284-60-9
cyclohexyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3-methyl-1-oxobutyl)amino-β-D-glucopyranoside

: 79284-53-0
N-((2R,3R,4R,5R,6R)-2-Cyclohexyloxy-4,5-bis-trimethylsilanyloxy-6-trimethylsilanyloxymethyl-tetrahydro-pyran-3-yl)-3-methyl-butyramide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Na, 2.) Dowex 50W resin / 1.) 48h, RT,

2: BSTFA / acetonitrile

With N,O-Bis(trimethylsilyl)trifluoroacetamide; Dowex 50W resin; sodium; In acetonitrile;
DOI:10.1016/S0040-4020(01)97937-2