methyl (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoate

Base Information

Chemical Name:methyl (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoate
CAS No.:433301-03-2
Molecular Formula:C₃₁H₄₃O₇P
Molecular Weight:558.652
Hs Code.:

Synonyms:methyl (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoate

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Chemical Property of methyl (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoate

Chemical Property:

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Technology Process of methyl (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoate

There total 3 articles about methyl (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7-(2,2-diphenylcyclopropyl)-6-(Z)-heptenal

: 433301-03-2
methyl (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran / -78 °C

1.2: tetrahydrofuran / -78 °C

2.1: 0.96 g / tetrahydrofuran / 20 °C

With lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ja0177399

Reference yield:

: 7-(2,2-diphenylcyclopropyl)-6-heptenoic acid

: 433301-03-2
methyl (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridinium chlorochromate / CH₂Cl₂ / 2 h / 20 °C

2.1: LDA / tetrahydrofuran / -78 °C

2.2: tetrahydrofuran / -78 °C

3.1: 0.96 g / tetrahydrofuran / 20 °C

With pyridinium chlorochromate; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja0177399