(2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoic acid

Base Information

Chemical Name:(2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoic acid
CAS No.:433301-06-5
Molecular Formula:C₃₀H₄₁O₇P
Molecular Weight:544.625
Hs Code.:

Synonyms:(2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoic acid

Chemical Property:

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Technology Process of (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoic acid

There total 4 articles about (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 433301-03-2
methyl (2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoate

: 433301-06-5
(2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoic acid

Guidance literature:: With sodium hydroxide; In ethanol; for 2h; Heating;
DOI:10.1021/ja0177399

Reference yield:

: 7-(2,2-diphenylcyclopropyl)-6-(Z)-heptenal

: 433301-06-5
(2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran / -78 °C

1.2: tetrahydrofuran / -78 °C

2.1: 0.96 g / tetrahydrofuran / 20 °C

3.1: aq. NaOH / ethanol / 2 h / Heating

With sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; ethanol;
DOI:10.1021/ja0177399

Reference yield:

: 7-(2,2-diphenylcyclopropyl)-6-heptenoic acid

: 433301-06-5
(2RS,3SR)-9-(2,2-diphenylcyclopropyl)-2-methyl-2-methoxy-3-diethylphosphoryloxy-8-nonenoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridinium chlorochromate / CH₂Cl₂ / 2 h / 20 °C

2.1: LDA / tetrahydrofuran / -78 °C

2.2: tetrahydrofuran / -78 °C

3.1: 0.96 g / tetrahydrofuran / 20 °C

4.1: aq. NaOH / ethanol / 2 h / Heating

With sodium hydroxide; pyridinium chlorochromate; lithium diisopropyl amide; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/ja0177399