tert-butyl {4-[1-(4-chlorophenyl)-2,2,2-trifluoro-1-hydroxyethyl]-phenyl}-carbamate

Base Information

Chemical Name:tert-butyl {4-[1-(4-chlorophenyl)-2,2,2-trifluoro-1-hydroxyethyl]-phenyl}-carbamate
CAS No.:1207471-79-1
Molecular Formula:C₁₉H₁₉ClF₃NO₃
Molecular Weight:401.813
Hs Code.:

Synonyms:tert-butyl {4-[1-(4-chlorophenyl)-2,2,2-trifluoro-1-hydroxyethyl]-phenyl}-carbamate

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Chemical Property of tert-butyl {4-[1-(4-chlorophenyl)-2,2,2-trifluoro-1-hydroxyethyl]-phenyl}-carbamate

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Technology Process of tert-butyl {4-[1-(4-chlorophenyl)-2,2,2-trifluoro-1-hydroxyethyl]-phenyl}-carbamate

There total 1 articles about tert-butyl {4-[1-(4-chlorophenyl)-2,2,2-trifluoro-1-hydroxyethyl]-phenyl}-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1207469-07-5
4-{1-(4-chlorophenyl)-2,2,2-trifluoro-1-[(trimethylsilyl)-oxy]ethyl}aniline

: 1207471-79-1
tert-butyl {4-[1-(4-chlorophenyl)-2,2,2-trifluoro-1-hydroxyethyl]-phenyl}-carbamate

Guidance literature:: di-tert-butyl dicarbonate; 4-{1-(4-chlorophenyl)-2,2,2-trifluoro-1-[(trimethylsilyl)-oxy]ethyl}aniline; With dmap; triethylamine; In tetrahydrofuran; at 20 ℃;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 5h;

With water; ammonium chloride; In tetrahydrofuran;

Reference yield:

: 1207471-79-1
tert-butyl {4-[1-(4-chlorophenyl)-2,2,2-trifluoro-1-hydroxyethyl]-phenyl}-carbamate

: 1207471-80-4
tert-butyl {4-[1-chloro-1-(4-chlorophenyl)-2,2,2-trifluoroethyl]-phenyl}carbamate.

Guidance literature:: tert-butyl {4-[1-(4-chlorophenyl)-2,2,2-trifluoro-1-hydroxyethyl]-phenyl}-carbamate; With pyridine; thionyl chloride; In toluene; at 70 ℃; for 8h;

With sodium hydrogencarbonate; In water; ethyl acetate; toluene;