bis(phenylselenato)zinc N,N,N',N'-tetramethylethylenediamine

Base Information

Chemical Name:bis(phenylselenato)zinc N,N,N',N'-tetramethylethylenediamine
CAS No.:290820-91-6
Molecular Formula:C₁₈H₂₆N₂Se₂Zn
Molecular Weight:493.728
Hs Code.:

Synonyms:bis(phenylselenato)zinc N,N,N',N'-tetramethylethylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(phenylselenato)zinc N,N,N',N'-tetramethylethylenediamine

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Technology Process of bis(phenylselenato)zinc N,N,N',N'-tetramethylethylenediamine

There total 3 articles about bis(phenylselenato)zinc N,N,N',N'-tetramethylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: bis(phenylselenolato) zinc

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 290820-91-6
bis(phenylselenato)zinc N,N,N',N'-tetramethylethylenediamine

Guidance literature:: With pyridine; heptane; In toluene; as suspn., stirred for 24 h; filtered, treated with pyridine, heptane, cooled to -24°C, XRD, elem. anal.;
DOI:10.1039/b002983l

Reference yield:

: 645-96-5
Benzeneselenol

: 290820-91-6
bis(phenylselenato)zinc N,N,N',N'-tetramethylethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: heptane / toluene

2: pyridine; heptane / toluene

With heptane; pyridine; In toluene;
DOI:10.1039/b002983l

Reference yield:

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 33861-17-5
phenyl trimethylsilyl selenide

: 557-34-6
zinc diacetate

: 290820-91-6
bis(phenylselenato)zinc N,N,N',N'-tetramethylethylenediamine

Guidance literature:: In tetrahydrofuran; under N2 atm. to Zn(OAc)2 in THF at 0°C TMEDA and PhSeSiMe3 were added; solvent was removed in vacuo, product was washed and dried;
DOI:10.1021/om050088v