C₃₅H₃₂O₁₀S

Base Information

• Chemical Name: C₃₅H₃₂O₁₀S
• CAS No.: 402483-41-4
• Molecular Formula: C₃₅H₃₂O₁₀S
• Molecular Weight: 644.699
• Mol file: 402483-41-4.mol

Synonyms:C₃₅H₃₂O₁₀S

Chemical Property of C₃₅H₃₂O₁₀S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₅H₃₂O₁₀S

There total 8 articles about C₃₅H₃₂O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-Mannose (530-26-7) → C35H32O10S (402483-41-4)

Guidance literature:

Multi-step reaction with 7 steps

1: PTSA / dimethylformamide

2: 70 percent / CrO₃-pyridine

3: 75 percent / PPh₃ / tetrahydrofuran

4: 65 percent / H₂ / Raney Ni / ethyl acetate

5: AcOH / H₂O

6: pyridine

7: pyridine

With pyridine; chromium trioxide-pyridine complex; hydrogen; toluene-4-sulfonic acid; acetic acid; triphenylphosphine; nickel; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(01)01906-2

Reference yield:

2,3:4,6-di-O-isopropylidene-D-mannopyranose (357604-61-6) → C35H32O10S (402483-41-4)

Guidance literature:

Multi-step reaction with 6 steps

1: 70 percent / CrO₃-pyridine

2: 75 percent / PPh₃ / tetrahydrofuran

3: 65 percent / H₂ / Raney Ni / ethyl acetate

4: AcOH / H₂O

5: pyridine

6: pyridine

With pyridine; chromium trioxide-pyridine complex; hydrogen; acetic acid; triphenylphosphine; nickel; In tetrahydrofuran; water; ethyl acetate;

DOI:10.1016/S0040-4039(01)01906-2

Reference yield:

2,3:4,6-Di-O-isopropylidene-D-mannopyranonolactone (143289-36-5) → C35H32O10S (402483-41-4)

Guidance literature:

Multi-step reaction with 5 steps

1: 75 percent / PPh₃ / tetrahydrofuran

2: 65 percent / H₂ / Raney Ni / ethyl acetate

3: AcOH / H₂O

4: pyridine

5: pyridine

With pyridine; hydrogen; acetic acid; triphenylphosphine; nickel; In tetrahydrofuran; water; ethyl acetate;

DOI:10.1016/S0040-4039(01)01906-2

upstream raw materials:

benzoyl chloride

D-Mannose

2,3:4,6-di-O-isopropylidene-D-mannopyranose

2,3:4,6-Di-O-isopropylidene-D-mannopyranonolactone

Downstream raw materials:

C₃₁H₃₀O₁₁S

C₃₁H₃₀O₉S

C₂₈H₂₅IO₇

Refernces