N N'-BIS-(5-BROMOSALICYLIDENE)ETHYLENE DIAMINE

Base Information

• Chemical Name: N N'-BIS-(5-BROMOSALICYLIDENE)ETHYLENE DIAMINE
• CAS No.: 17937-38-1
• Molecular Formula: C16H14 Br2 N2 O2
• Molecular Weight: 426.107
• Mol file: 17937-38-1.mol

Synonyms:N N-BIS-(5-BROMOSALICYLIDENE)ETHYLENE DIAMINE;N,N-Bis-(5-bromosalicylidene)ethylenediamine,97%

Chemical Property of N N'-BIS-(5-BROMOSALICYLIDENE)ETHYLENE DIAMINE

Chemical Property:

• Melting Point: 191-196 °C
• Refractive Index: 1.6220 (estimate)
• PSA: 58.20000
• Density: 1.6556 (rough estimate)
• LogP: 3.55060

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 36/37/38-22
• Safety Statements: 37/39-26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N N'-BIS-(5-BROMOSALICYLIDENE)ETHYLENE DIAMINE

There total 2 articles about N N'-BIS-(5-BROMOSALICYLIDENE)ETHYLENE DIAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

ethylenediamine (107-15-3,85404-18-8) + 5-bromosalicyclaldehyde (1761-61-1) → N,N'-bis(5-bromosalicylidene)ethane-1,2-diamine (17937-38-1)

Guidance literature:

In ethanol; at 20 ℃; for 0.333333h;

DOI:10.2174/157018010790596678

Reference yield:

→ N,N'-bis(5-bromosalicylidene)ethane-1,2-diamine (17937-38-1)

Guidance literature:

5-Brom-salicylaldehyd, Ethylendiamin;

Reference yield: 87.0%

N,N'-bis(5-bromosalicylidene)ethane-1,2-diamine (17937-38-1) → 2-((2-(5-bromo-2-hydroxybenzylamino)ethylamino)methyl)-4-bromophenol (162586-73-4)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 20 ℃; Reflux;

DOI:10.2174/157018010790596678

upstream raw materials:

ethylenediamine

5-bromosalicyclaldehyde

Downstream raw materials:

[TiO(salen(5-Br)2)]

Mn⁽³⁺⁾*C₁₆H₁₂Br₂N₂O₂^(2-)*O₂CCH₃^(1-) = [Mn(C₁₆H₁₂Br₂N₂O₂)(O₂CCH₃)]

Mn⁽³⁺⁾*C₁₆H₁₂Br₂N₂O₂^(2-)*O₂CC₃H₇^(1-) = [Mn(C₁₆H₁₂Br₂N₂O₂)(O₂CC₃H₇)]

Mn⁽³⁺⁾*C₁₆H₁₂Br₂N₂O₂^(2-)*O₂CCH₂C₆H₅^(1-) = [Mn(C₁₆H₁₂Br₂N₂O₂)(O₂CCH₂C₆H₅)]

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