2-monofluorododecane

Base Information

Chemical Name:2-monofluorododecane
CAS No.:114114-76-0
Molecular Formula:C₁₂H₂₅F
Molecular Weight:188.329
Hs Code.:

Synonyms:2-monofluorododecane

Suppliers and Price of 2-monofluorododecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-monofluorododecane

Chemical Property:

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Technology Process of 2-monofluorododecane

There total 2 articles about 2-monofluorododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114114-75-9
Methanesulfonic acid 1-methyl-undecyl ester

: 112-41-4,25067-08-7,62132-67-6
1-dodecene

: 1652-96-6
dodec-2-ene

: 114114-76-0
2-monofluorododecane

Guidance literature:: With tetrabutylammonium hydrogen bifluoride; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at 95 ℃; for 20h; Yield given;
DOI:10.1016/S0040-4039(00)96612-7

Reference yield:

: 112-41-4,25067-08-7,62132-67-6
1-dodecene

: 88-67-5
2-Iodobenzoic acid

: 1652-96-6
dodec-2-ene

: dodecan-2-yl 2-iodobenzoate

: 114114-76-0
2-monofluorododecane

Guidance literature:: With 1,1,2,2-tetramethyl-1,2-ethanediamino-N,N'-bis(3,5-di-tert-butylsalicylidene)-cobalt(II); 1,1,3,3-Tetramethyldisiloxane; 1-fluoro-2,4,6-trimethylpyridin-1-ium tetrafluoroborate; In ethyl acetate; at 20 ℃; for 18h; Inert atmosphere; Schlenk technique;
DOI:10.1021/jacs.9b01857

Reference yield: 99.0%

: 114114-76-0
2-monofluorododecane

: 13187-99-0
2-bromododecane

Guidance literature:: With dibromobis(cyclopentadienyl)titanium(IV); triethylaluminum; 1,1-dibromomethane; In hexane; at 20 ℃; for 0.5h;
DOI:10.1021/acs.orglett.5b02589