mono-p-phenyl ether of di(ethylene glycol)

Base Information

Chemical Name:mono-p-phenyl ether of di(ethylene glycol)
CAS No.:149704-56-3
Molecular Formula:C₃₇H₄₄O₃
Molecular Weight:536.755
Hs Code.:

mono-p-<bis(p-tert-butylphenyl)phenylmethyl>phenyl ether of di(ethylene glycol)

Synonyms:mono-p-phenyl ether of di(ethylene glycol)

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Chemical Property of mono-p-phenyl ether of di(ethylene glycol)

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Technology Process of mono-p-phenyl ether of di(ethylene glycol)

There total 9 articles about mono-p-phenyl ether of di(ethylene glycol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 628-89-7
2-(2-Chloroethoxy)ethanol

: Potassium; 4-[bis-(4-tert-butyl-phenyl)-phenyl-methyl]-phenolate

: 149704-56-3
mono-p-phenyl ether of di(ethylene glycol)

Guidance literature:: With potassium carbonate; In acetonitrile; for 120h; Heating;
DOI:10.1021/ja954334d

Reference yield:

: 102343-20-4
bis(4-tert-butylphenyl)phenyl-methanol

: 149704-56-3
mono-p-phenyl ether of di(ethylene glycol)

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / 24 h / Heating

2: KOH / butan-1-ol; H₂O / 36 h / Heating

3: 35percent HCl / CH₂Cl₂; methanol / 2.5 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; In methanol; dichloromethane; water; butan-1-ol;
DOI:10.1021/jo00066a030

Reference yield:

: 2-[2-(2-{4-[Bis-(4-tert-butyl-phenyl)-phenyl-methyl]-phenoxy}-ethoxy)-ethoxy]-tetrahydro-pyran

: 149704-56-3
mono-p-phenyl ether of di(ethylene glycol)

Guidance literature:: With hydrogenchloride; In methanol; dichloromethane; for 2.5h; Yield given; Ambient temperature;
DOI:10.1021/jo00066a030