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2-(2-Chloroethoxy)ethanol CAS NO.628-89-7 99%min
Cas No: 628-89-7
No Data 1 Kilogram 50 Metric Ton/Month CHANGZHOU HANGYU PHARMACEUTICAL TECHNOLOGY CO., LTD Contact Supplier
2-(2-Chloroethoxy)ethanol
Cas No: 628-89-7
No Data No Data Metric Ton/Day Changzhou Litong Chemical Co., Ltd. Contact Supplier
2-(2-Chloroethoxy)ethanol Manufacturer/High quality/Best price/In stock
Cas No: 628-89-7
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High quality 2-(2-Chloroethoxy) Ethanol supplier in China
Cas No: 628-89-7
No Data 1 Kilogram 30 Metric Ton/Month Simagchem Corporation Contact Supplier
2-(2-Chloroethoxy)ethanol
Cas No: 628-89-7
USD $ 12.0-12.0 / Gram 10 Gram 200 Metric Ton/Year Jinan Finer Chemical Co., Ltd Contact Supplier
Factory Supply 2-(2-chloroethoxy)ethanol
Cas No: 628-89-7
No Data 1 1 Ality Chemical Corporation Contact Supplier
2-(2-Chloroethoxy)ethanol
Cas No: 628-89-7
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
2-(2-Chloroethoxy)ethanol
Cas No: 628-89-7
No Data 1 Kilogram Unlimited Kilogram/Day Jiangxi LinQ Spices Co.,Ltd. Contact Supplier
2-(2-Chloroethoxy)ethanol CAS: 628-89-7
Cas No: 628-89-7
USD $ 1.0-2.0 / Metric Ton 5 Metric Ton 1000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
2-(2-Chloroethoxy)Ethanol with best price top supplier
Cas No: 628-89-7
USD $ 1.0-2.0 / Gram 10 Gram 200 Kilogram/Month Hubei Jusheng Technology Co., Ltd., Contact Supplier

628-89-7 Usage

Chemical Properties

colourless liquid

Uses

2-(2-Chloroethoxy)ethanol is a degradation product of Bis(2-Chloroethyl) Ether. 2-(2-Chloroethoxy)ethanol is a potential genotoxic impurity (PGI) in active pharmaceutical ingredients (APIs).
InChI:InChI=1/C4H9ClO2/c5-1-3-7-4-2-6/h6H,1-4H2

628-89-7 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A13074)  2-(2-Chloroethoxy)ethanol, 99%    628-89-7 50g 240.0CNY Detail
Alfa Aesar (A13074)  2-(2-Chloroethoxy)ethanol, 99%    628-89-7 250g 1012.0CNY Detail
Alfa Aesar (A13074)  2-(2-Chloroethoxy)ethanol, 99%    628-89-7 1000g 3288.0CNY Detail

628-89-7SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name 2-(2-Chloroethoxy)ethanol

1.2 Other means of identification

Product number -
Other names Diglycol Ch

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:628-89-7 SDS

628-89-7Synthetic route

oxirane
75-21-8

oxirane

2-chloro-ethanol
107-07-3

2-chloro-ethanol

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

Conditions
ConditionsYield
With sulfuric acid bei Siedetemperatur;
at 140℃;
With sulfuric acid
oxirane
75-21-8

oxirane

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

Conditions
ConditionsYield
With hydrogenchloride
ethylene glycol
107-21-1

ethylene glycol

2-chloro-ethanol
107-07-3

2-chloro-ethanol

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

Conditions
ConditionsYield
at 140℃; Erkalten mit HCl-Gas gesaettigt und Erhitzen auf 100grad;
ethylene glycol
107-21-1

ethylene glycol

2-chloro-ethanol
107-07-3

2-chloro-ethanol

A

2-(2-(2-(2-chloroethoxy)ethoxy)ethoxy)ethanol
5197-66-0

2-(2-(2-(2-chloroethoxy)ethoxy)ethoxy)ethanol

B

2-[2-(chloroethoxy)ethoxy]ethanol
5197-62-6

2-[2-(chloroethoxy)ethoxy]ethanol

C

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

Conditions
ConditionsYield
at 140℃;
2-(2-chloroethoxy)ethyl ethanoate
14258-40-3

2-(2-chloroethoxy)ethyl ethanoate

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

Conditions
ConditionsYield
With hydrogenchloride; methanol
diethylene glycol
111-46-6

diethylene glycol

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

Conditions
ConditionsYield
With pyridine; thionyl chloride
With hydrogenchloride; sulfuric acid; zinc(II) chloride at 160℃; for 7h;
1,4-dioxane
123-91-1

1,4-dioxane

A

2-(2-(2-(2-chloroethoxy)ethoxy)ethoxy)ethanol
5197-66-0

2-(2-(2-(2-chloroethoxy)ethoxy)ethoxy)ethanol

B

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

Conditions
ConditionsYield
With titanium tetrachloride 1.) 20 deg C, 2.) reflux, 7 d;A 150 mg
B 55 mg
2-chloromethyl-1,3-dioxolane
2568-30-1

2-chloromethyl-1,3-dioxolane

A

ethylene glycol
107-21-1

ethylene glycol

B

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

Conditions
ConditionsYield
With lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 0.2 h, 2.) Et2O, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
2-chloromethyl-1,3-dioxolane
2568-30-1

2-chloromethyl-1,3-dioxolane

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

Conditions
ConditionsYield
With lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 0.2 h, 2.) Et2O, 30 min; Yield given. Multistep reaction;
3-oxa-1,5-dichloropentane
111-44-4

3-oxa-1,5-dichloropentane

A

1,4-dioxane
123-91-1

1,4-dioxane

B

2-chloroethanal
107-20-0

2-chloroethanal

C

acetaldehyde
75-07-0

acetaldehyde

D

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

E

1,2-dichloro-ethane
107-06-2

1,2-dichloro-ethane

F

2-chloro-ethanol
107-07-3

2-chloro-ethanol

Conditions
ConditionsYield
In neat (no solvent) at 130 - 190℃; for 0.1h; Product distribution; thermal conversion; in presence of water, various time;
1-(2-Chloro-ethoxy)-2-nitrosooxy-ethane

1-(2-Chloro-ethoxy)-2-nitrosooxy-ethane

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

Conditions
ConditionsYield
With potassium chloride In 1,4-dioxane at 28℃; Rate constant; phosphate buffer pH 7.6;
oxirane
75-21-8

oxirane

sulfuric acid
7664-93-9

sulfuric acid

2-chloro-ethanol
107-07-3

2-chloro-ethanol

A

1,4-dioxane
123-91-1

1,4-dioxane

B

2-[2-(chloroethoxy)ethoxy]ethanol
5197-62-6

2-[2-(chloroethoxy)ethoxy]ethanol

C

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

2-chloro-ethanol
107-07-3

2-chloro-ethanol

A

1,4-dioxane
123-91-1

1,4-dioxane

B

2-[2-(chloroethoxy)ethoxy]ethanol
5197-62-6

2-[2-(chloroethoxy)ethoxy]ethanol

C

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

D

1,2-dichloro-ethane
107-06-2

1,2-dichloro-ethane

E

3-oxa-1,5-dichloropentane
111-44-4

3-oxa-1,5-dichloropentane

F

HCl, water

HCl, water

Conditions
ConditionsYield
at 150℃; for 5h; Product distribution; Kinetics; Rate constant; dependence of the products of ECH decomposition on temperature in sealed tube at 115, 130, 140, 150, 160 deg C;
2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

2-(2-azidoethoxy)ethanol
139115-90-5

2-(2-azidoethoxy)ethanol

Conditions
ConditionsYield
With sodium azide; sodium iodide In water at 60℃; for 96h;100%
With sodium azide In water at 80℃; for 16h; Inert atmosphere;99%
With sodium azide In water at 80℃; for 18h;99%
2,4,6-tris(benzyloxy)-1,3,5-triazine
7285-83-8

2,4,6-tris(benzyloxy)-1,3,5-triazine

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

benzyl (2-(2-chloroethoxy)ethyl) ether
64352-98-3

benzyl (2-(2-chloroethoxy)ethyl) ether

Conditions
ConditionsYield
With trifluorormethanesulfonic acid In 1,4-dioxane at 20℃; for 7h; Inert atmosphere;100%
2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

tert-butyl (4-(4-hydroxyphenyl)butyl)carbamate
465529-53-7

tert-butyl (4-(4-hydroxyphenyl)butyl)carbamate

C20H33NO5

C20H33NO5

Conditions
ConditionsYield
With potassium carbonate; potassium iodide In acetonitrile100%
4-hydroxy-4'-nitrobenzophenone
18920-70-2

4-hydroxy-4'-nitrobenzophenone

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

(4-(2-(2-hydroxyethoxy)ethoxy)phenyl)(4-nitrophenyl)methanone

(4-(2-(2-hydroxyethoxy)ethoxy)phenyl)(4-nitrophenyl)methanone

Conditions
ConditionsYield
With potassium carbonate; sodium iodide In N,N-dimethyl-formamide at 65 - 70℃; for 16h; Sealed tube;100%
2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}piperazine TFA salt

1-{2-[2-(2-azidoethoxy)ethoxy]ethyl}piperazine TFA salt

C14H29N5O4

C14H29N5O4

Conditions
ConditionsYield
With potassium carbonate; sodium iodide In acetonitrile Reflux;100%
2-(4-(dimethylamino)phenyl)-6-hydroxy-4H-chromen-4-one
887646-88-0

2-(4-(dimethylamino)phenyl)-6-hydroxy-4H-chromen-4-one

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

6-(2-(2-hydroxyethoxy)ethoxy)-4'-dimethylaminoflavone
1147337-36-7

6-(2-(2-hydroxyethoxy)ethoxy)-4'-dimethylaminoflavone

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 11h;99.3%
3,4-dihydro-2H-pyran
110-87-2

3,4-dihydro-2H-pyran

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

2-(2-(2-chloroethoxy)ethoxy)tetrahydro-2H-pyran
54533-84-5

2-(2-(2-chloroethoxy)ethoxy)tetrahydro-2H-pyran

Conditions
ConditionsYield
With hydrogenchloride99%
at 0 - 20℃; for 6h;99%
With hydrogenchloride at 20℃; for 1h; Etherification;98%
1,5-dihydroxynaphthalene
83-56-7

1,5-dihydroxynaphthalene

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

1,5-bis[2-(2-hydroxyethoxy)ethoxy]naphthalene
136133-14-7

1,5-bis[2-(2-hydroxyethoxy)ethoxy]naphthalene

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 82℃;99%
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 80℃; for 12h; Inert atmosphere;75%
With potassium carbonate In N,N-dimethyl-formamide Heating;67%
1,1'-biphenyl-3,3'-diol
612-76-0

1,1'-biphenyl-3,3'-diol

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

3,3'-bis(5-hydroxy-3-oxa-1-pentyloxy)-1,1'-biphenyl
929886-87-3

3,3'-bis(5-hydroxy-3-oxa-1-pentyloxy)-1,1'-biphenyl

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 24h;99%
tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

tert-butyl (2-(2-chloroethoxy)ethoxy)dimethylsilane
119382-85-3

tert-butyl (2-(2-chloroethoxy)ethoxy)dimethylsilane

Conditions
ConditionsYield
With 1H-imidazole In tetrahydrofuran at 0 - 20℃; for 16h;99%
With 1H-imidazole In acetonitrile at 20℃;92%
2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

1,8-diazabicyclo[5.4.0]undec-7-ene
6674-22-2

1,8-diazabicyclo[5.4.0]undec-7-ene

1-[2-(2-hydroxyethoxy)ethyl]-1,8-diazabicyclo[5.4.0]undec-7-ene chloride

1-[2-(2-hydroxyethoxy)ethyl]-1,8-diazabicyclo[5.4.0]undec-7-ene chloride

Conditions
ConditionsYield
In acetonitrile at 75℃; for 24h; Inert atmosphere;99%
In ethyl acetate at 80℃; for 24h; Inert atmosphere;95%
11-piperazin-1-yldibenzo[b,f][1,4]thiazepine hydrochloride
753475-15-9

11-piperazin-1-yldibenzo[b,f][1,4]thiazepine hydrochloride

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

Quetiapine
111974-69-7

Quetiapine

Conditions
ConditionsYield
With sodium carbonate; sodium iodide; tetrabutylammomium bromide In toluene at 115 - 120℃; for 17h; Heating / reflux;98.2%
With sodium carbonate; sodium iodide; tetrabutylammomium bromide In butan-1-ol at 115 - 120℃; for 17h; Heating / reflux;96.9%
With sodium carbonate; sodium iodide In butan-1-ol at 115 - 120℃; for 17h; Heating / reflux;94.1%
benzene-1,2-diol
120-80-9

benzene-1,2-diol

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

1,2-bis[2-(2-hydroxyethoxy)ethoxy]benzene
41757-99-7

1,2-bis[2-(2-hydroxyethoxy)ethoxy]benzene

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 100℃; for 12h; Inert atmosphere;98%
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 75℃; for 72h;88.4%
Stage #1: benzene-1,2-diol With potassium carbonate In N,N-dimethyl-formamide at 90℃; Inert atmosphere;
Stage #2: 2-(2-Chloroethoxy)ethanol With potassium iodide In N,N-dimethyl-formamide at 100℃; for 144h; Inert atmosphere;
85.5%
2,2'-dihydroxybiphenyl
1806-29-7

2,2'-dihydroxybiphenyl

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

2,2'-bis(5-hydroxy-3-oxa-1-pentyloxy)-1,1'-biphenyl
91859-84-6

2,2'-bis(5-hydroxy-3-oxa-1-pentyloxy)-1,1'-biphenyl

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 24h;98%
2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

methyl 4-hydroxylbenzoate
99-76-3

methyl 4-hydroxylbenzoate

methyl 4-[2-(2-hydroxyethoxy)ethoxy]-benzoate
159550-14-8

methyl 4-[2-(2-hydroxyethoxy)ethoxy]-benzoate

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide Reflux;98%
With potassium carbonate; potassium iodide In cyclohexanone for 24h; Inert atmosphere; Reflux;66%
With caesium carbonate; potassium iodide In cyclohexanone for 24h; Reflux;
With caesium carbonate; potassium iodide for 24h; Reflux;
2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

benzyl alcohol
100-51-6

benzyl alcohol

benzyl (2-(2-chloroethoxy)ethyl) ether
64352-98-3

benzyl (2-(2-chloroethoxy)ethyl) ether

Conditions
ConditionsYield
With [bis(trifluoromethanesulfonyl)imidate](triphenylphosphine)gold (I) at 150℃; for 0.5h; Inert atmosphere; Microwave irradiation;98%
N-methyl-perfluorobutane-1-sulfonamide
68298-12-4

N-methyl-perfluorobutane-1-sulfonamide

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

C9H12F9NO4S

C9H12F9NO4S

Conditions
ConditionsYield
With potassium carbonate at 90 - 120℃; for 17.25h;97.8%
2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

m-bis(2-(p-hydroxyphenyl)-1,10-phenanthrolinyl)benzene
159726-86-0

m-bis(2-(p-hydroxyphenyl)-1,10-phenanthrolinyl)benzene

2-[2-(4-{9-[3-(9-{4-[2-(2-Hydroxy-ethoxy)-ethoxy]-phenyl}-[1,10]phenanthrolin-2-yl)-phenyl]-[1,10]phenanthrolin-2-yl}-phenoxy)-ethoxy]-ethanol

2-[2-(4-{9-[3-(9-{4-[2-(2-Hydroxy-ethoxy)-ethoxy]-phenyl}-[1,10]phenanthrolin-2-yl)-phenyl]-[1,10]phenanthrolin-2-yl}-phenoxy)-ethoxy]-ethanol

Conditions
ConditionsYield
With caesium carbonate In N,N-dimethyl-formamide at 80℃;97%
With caesium carbonate 1.) DMF, 80 deg C, 1 h, 2.) DMF, 80 deg C, 6 h; Yield given; Multistep reaction;
2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

chlorophosphoric acid diphenyl ester
2524-64-3

chlorophosphoric acid diphenyl ester

2-(2-chloro-ethoxy)-ethyldiphenylphosphate
1232681-87-6

2-(2-chloro-ethoxy)-ethyldiphenylphosphate

Conditions
ConditionsYield
With molybdenum(VI) tetrachloride oxide; triethylamine In dichloromethane at 20℃; for 1h;97%
4-(4,6-diphenoxy-1,3,5-triazine-2-yl)-4-benzylmorpholinium trifluoromethanesulfonate

4-(4,6-diphenoxy-1,3,5-triazine-2-yl)-4-benzylmorpholinium trifluoromethanesulfonate

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

benzyl (2-(2-chloroethoxy)ethyl) ether
64352-98-3

benzyl (2-(2-chloroethoxy)ethyl) ether

Conditions
ConditionsYield
With magnesium oxide In 1,2-dimethoxyethane at 20℃; for 2h; Inert atmosphere;97%
2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

1-[2-(2-hydroxyethoxy)ethyl]-1,5-diazabicyclo[4.3.0]non-5-ene chloride

1-[2-(2-hydroxyethoxy)ethyl]-1,5-diazabicyclo[4.3.0]non-5-ene chloride

Conditions
ConditionsYield
In ethyl acetate at 80℃; for 24h; Inert atmosphere;97%
6-(4-(3,3,4,4,5,5,6,6,6-nonafluorohexyl)benzyloxy)-1,3,5-triazine-2,4(1H,3H)-dione

6-(4-(3,3,4,4,5,5,6,6,6-nonafluorohexyl)benzyloxy)-1,3,5-triazine-2,4(1H,3H)-dione

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

4-(3,3,4,4,5,5,6,6,6-nonafluorohexyl)benzyl 2-(2-chloroethoxy)ethyl ether

4-(3,3,4,4,5,5,6,6,6-nonafluorohexyl)benzyl 2-(2-chloroethoxy)ethyl ether

Conditions
ConditionsYield
With trifluorormethanesulfonic acid In 1,4-dioxane at 20℃; for 5h; Molecular sieve;97%
1,4-bis[2-(4-hydroxyphenyl)-2-propylene]benzene
4084-45-1

1,4-bis[2-(4-hydroxyphenyl)-2-propylene]benzene

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

2-(2-{4''-[2-(2-hydroxy-ethoxy)-ethoxy]-[1,1';4',1'']terphenyl-4-yloxy}-ethoxy)-ethanol

2-(2-{4''-[2-(2-hydroxy-ethoxy)-ethoxy]-[1,1';4',1'']terphenyl-4-yloxy}-ethoxy)-ethanol

Conditions
ConditionsYield
With potassium carbonate; lithium bromide In N,N-dimethyl-formamide96%
1-(3-hydroxyphenyl)pentan-1-one
62810-51-9

1-(3-hydroxyphenyl)pentan-1-one

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

1-(3-((2-((2-hydroxyethyl)oxy)ethyl)oxy)phenyl)-1-pentanone

1-(3-((2-((2-hydroxyethyl)oxy)ethyl)oxy)phenyl)-1-pentanone

Conditions
ConditionsYield
With potassium carbonate In acetone for 60h; Heating / reflux;96%
4-Cyano-4'-hydroxybiphenyl
19812-93-2

4-Cyano-4'-hydroxybiphenyl

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

C17H17NO3
127972-30-9

C17H17NO3

Conditions
ConditionsYield
With potassium phosphate In dimethyl sulfoxide at 110℃; for 12h;96%
piperazine
110-85-0

piperazine

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

1-[2-(2-hydroxyethoxy)ethyl]piperazine
13349-82-1

1-[2-(2-hydroxyethoxy)ethyl]piperazine

Conditions
ConditionsYield
With piperazine dihydrochloride In ethanol for 10h; Reflux; Large scale;95.1%
at 120 - 140℃; for 1h;70%
5-tert-butyl-N,N'-bis(3-hydroxyphenyl)-1,3-benzenediamide
835875-06-4

5-tert-butyl-N,N'-bis(3-hydroxyphenyl)-1,3-benzenediamide

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

5-tert-butyl-N,N'-bis-{3-[2-(2-hydroxyethoxy)ethoxy]phenyl}-1,3-benzenediamide
835875-09-7

5-tert-butyl-N,N'-bis-{3-[2-(2-hydroxyethoxy)ethoxy]phenyl}-1,3-benzenediamide

Conditions
ConditionsYield
With potassium carbonate In acetonitrile for 120h; Heating;95%
1-(3-hydroxyphenyl)propan-1-one
13103-80-5

1-(3-hydroxyphenyl)propan-1-one

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

1-(3-((2-((2-hydroxyethyl)oxy)ethyl)oxy)phenyl)-1-propanone

1-(3-((2-((2-hydroxyethyl)oxy)ethyl)oxy)phenyl)-1-propanone

Conditions
ConditionsYield
With potassium carbonate In acetone for 60h; Heating / reflux;95%
11-piperazin-1-yldibenzo[b,f][1,4]thiazepine hydrochloride
753475-15-9

11-piperazin-1-yldibenzo[b,f][1,4]thiazepine hydrochloride

2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

(2E)-but-2-enedioic acid
110-17-8

(2E)-but-2-enedioic acid

quetiapine fumarate

quetiapine fumarate

Conditions
ConditionsYield
Stage #1: 11-piperazin-1-yldibenzo[b,f][1,4]thiazepine hydrochloride; 2-(2-Chloroethoxy)ethanol With sodium carbonate; sodium iodide In propan-1-ol; N,N-dimethyl-formamide at 10 - 20℃; for 24h; Heating / reflux;
Stage #2: (2E)-but-2-enedioic acid In ethanol
95%
Stage #1: 11-piperazin-1-yldibenzo[b,f][1,4]thiazepine hydrochloride; 2-(2-Chloroethoxy)ethanol With sodium carbonate; sodium iodide In 1-methyl-pyrrolidin-2-one; propan-1-ol for 24h; Heating / reflux;
Stage #2: (2E)-but-2-enedioic acid In ethanol
2-(2-Chloroethoxy)ethanol
628-89-7

2-(2-Chloroethoxy)ethanol

2-(2-mercaptoethoxy)ethanol
17643-17-3

2-(2-mercaptoethoxy)ethanol

Conditions
ConditionsYield
Stage #1: 2-(2-Chloroethoxy)ethanol With thiourea; sodium iodide In acetonitrile at 20℃; for 72h; Reflux;
Stage #2: With water; sodium hydroxide In ethanol for 24h; Reflux;
95%
Stage #1: 2-(2-Chloroethoxy)ethanol With thiourea In water at 100℃; for 18h; Inert atmosphere;
Stage #2: With sodium hydroxide In water at 20 - 100℃;
Stage #3: With hydrogenchloride In water pH=4; Inert atmosphere; Cooling with ice;
49%
With thiourea
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