(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-1,3-dihydroxypentane

Base Information

Chemical Name:(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-1,3-dihydroxypentane
CAS No.:115654-51-8
Molecular Formula:C₁₆H₃₁NO₄
Molecular Weight:301.426
Hs Code.:

Synonyms:(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-1,3-dihydroxypentane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-1,3-dihydroxypentane

Chemical Property:

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Technology Process of (3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-1,3-dihydroxypentane

There total 6 articles about (3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-1,3-dihydroxypentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7722-84-1
dihydrogen peroxide

: 280-64-8
9-bora-bicyclo[3.3.1]nonane

: 104856-06-6
tert-butyl [(1S,2S)-1-(cyclohexylmethyl)-2-hydroxy-3-butenyl]carbamate

: 115654-51-8
(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-1,3-dihydroxypentane

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; chloroform; water; ethyl acetate;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 115654-51-8
(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-1,3-dihydroxypentane

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CH₂Cl₂ / 4 h / Ambient temperature

2: 1) 9-BBN, 2) 30percent H₂O₂, aq. NaOH / 1) THF, r.t., 3 h, 2) 50 deg C, 90 min

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; In dichloromethane;
DOI:10.1021/jm00126a038

Reference yield:

: 104856-09-9
(3S,4S)-4-amino-5-cyclohexyl-3-hydroxy-1-pentene

: 115654-51-8
(3S,4S)-4-<(tert-butyloxycarbonyl)amino>-5-cyclohexyl-1,3-dihydroxypentane

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CH₂Cl₂ / 4 h / Ambient temperature

2: 1) 9-BBN, 2) 30percent H₂O₂, aq. NaOH / 1) THF, r.t., 3 h, 2) 50 deg C, 90 min

With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide; In dichloromethane;
DOI:10.1021/jm00126a038