C₂₁H₂₁FN₂O₅S

Base Information

Chemical Name:C₂₁H₂₁FN₂O₅S
CAS No.:1374229-64-7
Molecular Formula:C₂₁H₂₁FN₂O₅S
Molecular Weight:432.473
Hs Code.:

C<sub>21</sub>H<sub>21</sub>FN<sub>2</sub>O<sub>5</sub>S

Synonyms:C₂₁H₂₁FN₂O₅S

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Chemical Property of C₂₁H₂₁FN₂O₅S

Chemical Property:

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Technology Process of C₂₁H₂₁FN₂O₅S

There total 7 articles about C₂₁H₂₁FN₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₁₇ClFNO₄S

: 593-56-6
N-methoxylamine hydrochloride

: 1374229-64-7
C₂₁H₂₁FN₂O₅S

Guidance literature:: With pyridine; at 100 ℃; for 1.5h;

Reference yield:

: 691857-46-2
ethyl 2-(4-fluorophenyl)-5-hydroxy-6-nitrobenzofuran-3-carboxylate

: 1374229-64-7
C₂₁H₂₁FN₂O₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

2.1: triethylamine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 1 h / 20 °C / Inert atmosphere

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 1.5 h / 20 °C

4.1: pyridine / dmap / dichloromethane / 2 h / 0 - 20 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

6.1: lithium hydroxide / tetrahydrofuran; methanol / 2 h / 70 °C

6.2: 20 °C

7.1: thionyl chloride / 2 h / 80 °C

8.1: pyridine / 1.5 h / 100 °C

With pyridine; thionyl chloride; hydrogen; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; mineral oil;

Reference yield:

: 691857-07-5
ethyl 2-(4-fluorophenyl)-5-isopropoxy-6-nitrobenzofuran-3-carboxylate

: 1374229-64-7
C₂₁H₂₁FN₂O₅S

Guidance literature:: Multi-step reaction with 9 steps

1.1: boron trichloride / dichloromethane / 1 h / 0 - 20 °C

1.2: Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

3.1: triethylamine / bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / 1 h / 20 °C / Inert atmosphere

4.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 1.5 h / 20 °C

5.1: pyridine / dmap / dichloromethane / 2 h / 0 - 20 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere

7.1: lithium hydroxide / tetrahydrofuran; methanol / 2 h / 70 °C

7.2: 20 °C

8.1: thionyl chloride / 2 h / 80 °C

9.1: pyridine / 1.5 h / 100 °C

With pyridine; thionyl chloride; hydrogen; boron trichloride; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; mineral oil;