Sodium N-(2-thienylmethyl)-4-cyclohexylsulfonyl-5-sulfamoyl-orthanilate

Base Information

Chemical Name:Sodium N-(2-thienylmethyl)-4-cyclohexylsulfonyl-5-sulfamoyl-orthanilate
CAS No.:85958-46-9
Molecular Formula:C₁₇H₂₁N₂O₇S₄*Na
Molecular Weight:516.617
Hs Code.:

Synonyms:Sodium N-(2-thienylmethyl)-4-cyclohexylsulfonyl-5-sulfamoyl-orthanilate

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Chemical Property of Sodium N-(2-thienylmethyl)-4-cyclohexylsulfonyl-5-sulfamoyl-orthanilate

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Technology Process of Sodium N-(2-thienylmethyl)-4-cyclohexylsulfonyl-5-sulfamoyl-orthanilate

There total 7 articles about Sodium N-(2-thienylmethyl)-4-cyclohexylsulfonyl-5-sulfamoyl-orthanilate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(2-thienylmethyl)-4-cyclohexylsulfonyl-5-sulfamoyl-orthanilic acid phenyl ester

: 85958-46-9
Sodium N-(2-thienylmethyl)-4-cyclohexylsulfonyl-5-sulfamoyl-orthanilate

Guidance literature:: With sodium hydroxide; at 95 ℃; for 1h;
DOI:10.1021/jm00362a017

Reference yield:

: 27757-85-3
2-Aminomethylthiophene

: 85958-46-9
Sodium N-(2-thienylmethyl)-4-cyclohexylsulfonyl-5-sulfamoyl-orthanilate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.5 h / 90 °C

2: 85percent 3-chloroperbenzoic acid / CH₂Cl₂ / 3 h / Ambient temperature

3: 2N aq. NaOH / 1 h / 95 °C

With sodium hydroxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00362a017

Reference yield:

: 1569-69-3
Cyclohexanethiol

: 85958-46-9
Sodium N-(2-thienylmethyl)-4-cyclohexylsulfonyl-5-sulfamoyl-orthanilate

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / K₂CO₃ / dimethylformamide / 1 h / 115 °C

2: 1.5 h / 90 °C

3: 85percent 3-chloroperbenzoic acid / CH₂Cl₂ / 3 h / Ambient temperature

4: 2N aq. NaOH / 1 h / 95 °C

With sodium hydroxide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00362a017