C₆₁H₁₁₆N₂O₁₂Si₃

Base Information

Chemical Name:C₆₁H₁₁₆N₂O₁₂Si₃
CAS No.:1262536-17-3
Molecular Formula:C₆₁H₁₁₆N₂O₁₂Si₃
Molecular Weight:1153.85
Hs Code.:

C<sub>61</sub>H<sub>116</sub>N<sub>2</sub>O<sub>12</sub>Si<sub>3</sub>

Synonyms:C₆₁H₁₁₆N₂O₁₂Si₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₁H₁₁₆N₂O₁₂Si₃

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Technology Process of C₆₁H₁₁₆N₂O₁₂Si₃

There total 9 articles about C₆₁H₁₁₆N₂O₁₂Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1262536-13-9
C₆₁H₁₁₈N₂O₁₃Si₃

: 1262536-17-3
C₆₁H₁₁₆N₂O₁₂Si₃

Guidance literature:: C₆₁H₁₁₈N₂O₁₃Si₃; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran;

With dmap; In tetrahydrofuran; toluene; Reflux;
DOI:10.1021/ml100252s

Reference yield:

: C₆₅H₁₂₄N₂O₁₄Si₃

: 1262536-17-3
C₆₁H₁₁₆N₂O₁₂Si₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tris(acetoxy)borohydride / water

2.1: water; lithium hydroxide / tetrahydrofuran; ethanol

3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran

3.2: Reflux

With 2,4,6-trichlorobenzoyl chloride; water; sodium tris(acetoxy)borohydride; triethylamine; lithium hydroxide; In tetrahydrofuran; ethanol; water; 3.1: Yamaguchi's macrolactonization / 3.2: Yamaguchi's macrolactonization;
DOI:10.1021/ml100252s

Reference yield:

: 497832-22-1
(9S)-9,2',4''-O-tris(triethylsilyl)-9-dihydroerythromycin A

: 1262536-17-3
C₆₁H₁₁₆N₂O₁₂Si₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: lead(IV) tetraacetate / dichloromethane

2.1: sodium tris(acetoxy)borohydride

3.1: sodium tris(acetoxy)borohydride / water

4.1: water; lithium hydroxide / tetrahydrofuran; ethanol

5.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran

5.2: Reflux

With 2,4,6-trichlorobenzoyl chloride; water; lead(IV) tetraacetate; sodium tris(acetoxy)borohydride; triethylamine; lithium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; 5.1: Yamaguchi's macrolactonization / 5.2: Yamaguchi's macrolactonization;
DOI:10.1021/ml100252s