(4,5-dimethoxy-2-nitrophenyl)methanamine

Base Information

Chemical Name:(4,5-dimethoxy-2-nitrophenyl)methanamine
CAS No.:123330-73-4
Molecular Formula:C₉H₁₂N₂O₄
Molecular Weight:212.205
Hs Code.:

Synonyms:(4,5-dimethoxy-2-nitrophenyl)methanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4,5-dimethoxy-2-nitrophenyl)methanamine

Chemical Property:

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Technology Process of (4,5-dimethoxy-2-nitrophenyl)methanamine

There total 7 articles about (4,5-dimethoxy-2-nitrophenyl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 288591-59-3
4,5-dimethoxy-2-nitrobenzaldehyde oxime acetate

: 123330-73-4
(4,5-dimethoxy-2-nitrophenyl)methanamine

Guidance literature:: With borane; In tetrahydrofuran; for 24h; Heating;
DOI:10.1021/jo9917846

Reference yield:

: 35970-04-8
4,5-dimethoxy-2-nitrobenzyl phthalimide

: 123330-73-4
(4,5-dimethoxy-2-nitrophenyl)methanamine

Guidance literature:: With ethanol; hydrazine hydrate; anschliessend mit konz. wss.HCl;
DOI:10.1021/ja01163a070

Reference yield:

: 29577-51-3
2-nitro-4,5-dimethoxybenzaldehyde oxime

: 123330-73-4
(4,5-dimethoxy-2-nitrophenyl)methanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Et₃N / CH₂Cl₂ / 2 h

2: 35 percent / BH₃ / tetrahydrofuran / 24 h / Heating

With borane; triethylamine; In tetrahydrofuran; dichloromethane; 1: Acetylation / 2: Reduction;
DOI:10.1021/jo9917846