2-(2-biphenyl-4-ylethyl)tetrahydrothiophene-2-carboxylic acid 1,1-dioxide

Base Information

Chemical Name:2-(2-biphenyl-4-ylethyl)tetrahydrothiophene-2-carboxylic acid 1,1-dioxide
CAS No.:1354546-69-2
Molecular Formula:C₁₉H₂₀O₄S
Molecular Weight:344.431
Hs Code.:

Synonyms:2-(2-biphenyl-4-ylethyl)tetrahydrothiophene-2-carboxylic acid 1,1-dioxide

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Chemical Property of 2-(2-biphenyl-4-ylethyl)tetrahydrothiophene-2-carboxylic acid 1,1-dioxide

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Technology Process of 2-(2-biphenyl-4-ylethyl)tetrahydrothiophene-2-carboxylic acid 1,1-dioxide

There total 3 articles about 2-(2-biphenyl-4-ylethyl)tetrahydrothiophene-2-carboxylic acid 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1354546-29-4
ethyl 2-(2-biphenyl-4-ylethyl)tetrahydrothiophene-2-carboxylate 1,1-dioxide

: 1354546-69-2
2-(2-biphenyl-4-ylethyl)tetrahydrothiophene-2-carboxylic acid 1,1-dioxide

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃;
DOI:10.1021/jm2014748

Reference yield:

: 18342-43-3
1,1-dioxo-tetrahydro-1λ⁶-thiophene-2-carboxylic acid ethyl ester

: 1354546-69-2
2-(2-biphenyl-4-ylethyl)tetrahydrothiophene-2-carboxylic acid 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 14 h

2: lithium hydroxide / tetrahydrofuran; methanol; water / 20 °C

With caesium carbonate; lithium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm2014748

Reference yield:

: 178685-10-4
4-(2-iodoethyl)-1,1'-biphenyl

: 1354546-69-2
2-(2-biphenyl-4-ylethyl)tetrahydrothiophene-2-carboxylic acid 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide / 14 h

2: lithium hydroxide / tetrahydrofuran; methanol; water / 20 °C

With caesium carbonate; lithium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jm2014748