N-(4-(((2-cyanobenzo[d]thiazol-6-yl)oxy)methyl)phenyl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

Base Information

Chemical Name:N-(4-(((2-cyanobenzo[d]thiazol-6-yl)oxy)methyl)phenyl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide
CAS No.:1426551-44-1
Molecular Formula:C₂₉H₂₇N₃O₄S
Molecular Weight:513.617
Hs Code.:

Synonyms:N-(4-(((2-cyanobenzo[d]thiazol-6-yl)oxy)methyl)phenyl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

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Chemical Property of N-(4-(((2-cyanobenzo[d]thiazol-6-yl)oxy)methyl)phenyl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

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Technology Process of N-(4-(((2-cyanobenzo[d]thiazol-6-yl)oxy)methyl)phenyl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

There total 6 articles about N-(4-(((2-cyanobenzo[d]thiazol-6-yl)oxy)methyl)phenyl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426551-43-0
N-(4-(bromomethyl)phenyl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

: 939-69-5
2-cyano-6-hydroxybenzothiazole

: 1426551-44-1
N-(4-(((2-cyanobenzo[d]thiazol-6-yl)oxy)methyl)phenyl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

Guidance literature:: With 2,4,6-trimethyl-pyridine; silver carbonate; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 1426551-42-9
N-(4-(hydroxymethyl)phenyl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

: 1426551-44-1
N-(4-(((2-cyanobenzo[d]thiazol-6-yl)oxy)methyl)phenyl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; carbon tetrabromide / dichloromethane / 3 h / 0 - 20 °C

2: 2,4,6-trimethyl-pyridine; silver carbonate / tetrahydrofuran / 20 °C

With 2,4,6-trimethyl-pyridine; carbon tetrabromide; triphenylphosphine; silver carbonate; In tetrahydrofuran; dichloromethane;

Reference yield:

: 700-13-0
Trimethylhydroquinone

: 1426551-44-1
N-(4-(((2-cyanobenzo[d]thiazol-6-yl)oxy)methyl)phenyl)-3-methyl-3-(2,4,5-trimethyl-3,6-dioxocyclohexa-1,4-dien-1-yl)butanamide

Guidance literature:: Multi-step reaction with 5 steps

1: methanesulfonic acid / 2 h / 70 °C

2: N-Bromosuccinimide; water / acetonitrile; acetone / 0.5 h / 20 °C

3: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.5 h / 0 °C

4: triphenylphosphine; carbon tetrabromide / dichloromethane / 3 h / 0 - 20 °C

5: 2,4,6-trimethyl-pyridine; silver carbonate / tetrahydrofuran / 20 °C

With 4-methyl-morpholine; 2,4,6-trimethyl-pyridine; N-Bromosuccinimide; methanesulfonic acid; carbon tetrabromide; water; triphenylphosphine; silver carbonate; isobutyl chloroformate; In tetrahydrofuran; dichloromethane; acetone; acetonitrile;