1,1-dideuterio-N-(1-deuterio-1-(4-fluorophenyl)ethyl)-N-(2-deuteriobenzyl)ethanamine

Base Information

• Chemical Name: 1,1-dideuterio-N-(1-deuterio-1-(4-fluorophenyl)ethyl)-N-(2-deuteriobenzyl)ethanamine
• CAS No.: 1224733-38-3
• Molecular Formula: C₁₇H₂₀FN
• Molecular Weight: 261.319

Synonyms:1,1-dideuterio-N-(1-deuterio-1-(4-fluorophenyl)ethyl)-N-(2-deuteriobenzyl)ethanamine

Chemical Property of 1,1-dideuterio-N-(1-deuterio-1-(4-fluorophenyl)ethyl)-N-(2-deuteriobenzyl)ethanamine

Chemical Property:

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Technology Process of 1,1-dideuterio-N-(1-deuterio-1-(4-fluorophenyl)ethyl)-N-(2-deuteriobenzyl)ethanamine

There total 2 articles about 1,1-dideuterio-N-(1-deuterio-1-(4-fluorophenyl)ethyl)-N-(2-deuteriobenzyl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-iodobenzyl)-N,N'-bis(2,2-dideuterioethyl)amine (1224733-21-4) + N-ethyl-N-(2-iodobenzyl)ethanamine (99558-03-9) + 4-flourophenylmagnesium bromide (352-13-6) → N-benzyl-N-ethyl-1-(4-fluorophenyl)ethanamine (1224733-27-0) + 1,1-dideuterio-N-(1-deuterio-1-(4-fluorophenyl)ethyl)-N-(2-deuteriobenzyl)ethanamine (1224733-38-3)

Guidance literature:

With iron(III)-acetylacetonate; In diethyl ether; tert-butyl methyl ether; at 20 ℃; Inert atmosphere;

Reference yield:

N-(2-iodobenzyl)-N,N'-bis(2,2-dideuterioethyl)amine (1224733-21-4) + 4-flourophenylmagnesium bromide (352-13-6) + 2-(piperidin-1-ylmethyl)phenyl iodide (76464-88-5) → N-benzyl-2-(4-fluorophenyl)piperidine (1355201-70-5) + 1,1-dideuterio-N-(1-deuterio-1-(4-fluorophenyl)ethyl)-N-(2-deuteriobenzyl)ethanamine (1224733-38-3)

Guidance literature:

With iron(III)-acetylacetonate; In diethyl ether; tert-butyl methyl ether; at 50 ℃; Inert atmosphere;

upstream raw materials:

N-(2-iodobenzyl)-N,N'-bis(2,2-dideuterioethyl)amine

N-ethyl-N-(2-iodobenzyl)ethanamine

4-flourophenylmagnesium bromide

2-(piperidin-1-ylmethyl)phenyl iodide

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