1-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-chloro-2,4-dihydroxy benzoate

Base Information

Chemical Name:1-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-chloro-2,4-dihydroxy benzoate
CAS No.:854261-06-6
Molecular Formula:C₂₂H₂₆ClNO₁₀
Molecular Weight:499.902
Hs Code.:

Synonyms:1-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-chloro-2,4-dihydroxy benzoate

Suppliers and Price of 1-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-chloro-2,4-dihydroxy benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-chloro-2,4-dihydroxy benzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-chloro-2,4-dihydroxy benzoate

There total 9 articles about 1-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-chloro-2,4-dihydroxy benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 854261-02-2
1-(2-methoxy-3,6-bis(methoxymethoxy)phenyl)propan-2-ol

: 854261-06-6
1-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-chloro-2,4-dihydroxy benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: NH₄NO₃; (CF₃CO)2O / acetonitrile / 0.25 h / 20 °C

1.2: LiOH / tetrahydrofuran; methanol; H₂O / 0.08 h

2.1: DMAP; DCC / dimethylformamide; tetrahydrofuran / 12 h / 50 °C

3.1: H₂ / PtO₂ / ethanol / 12 h / 20 °C

4.1: CH₂Cl₂ / 12 h / 30 °C

With ammonium nitrate; dmap; hydrogen; dicyclohexyl-carbodiimide; trifluoroacetic anhydride; platinum(IV) oxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo061054f

Reference yield:

: 854261-03-3
1-(2-methoxy-3,6-bis(methoxymethoxy)-5-nitrophenyl)propan-2-ol

: 854261-06-6
1-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-chloro-2,4-dihydroxy benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: DMAP; DCC / dimethylformamide; tetrahydrofuran / 12 h / 50 °C

2: H₂ / PtO₂ / ethanol / 12 h / 20 °C

3: CH₂Cl₂ / 12 h / 30 °C

With dmap; hydrogen; dicyclohexyl-carbodiimide; platinum(IV) oxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo061054f

Reference yield:

: 854261-04-4
1-(2-methoxy-3,6-bis(methoxymethoxy)-5-nitrophenyl)propan-2-yl 5-chloro-2,4-dihydroxy benzoate

: 854261-06-6
1-(3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenyl)propan-2-yl 5-chloro-2,4-dihydroxy benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / PtO₂ / ethanol / 12 h / 20 °C

2: CH₂Cl₂ / 12 h / 30 °C

With hydrogen; platinum(IV) oxide; In ethanol; dichloromethane;
DOI:10.1021/jo061054f