4-chloro-2-allylbenzonitrile

Base Information

Chemical Name:4-chloro-2-allylbenzonitrile
CAS No.:1244549-41-4
Molecular Formula:C₁₀H₈ClN
Molecular Weight:177.633
Hs Code.:

Synonyms:4-chloro-2-allylbenzonitrile

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Chemical Property of 4-chloro-2-allylbenzonitrile

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Technology Process of 4-chloro-2-allylbenzonitrile

There total 2 articles about 4-chloro-2-allylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 57381-49-4
2-bromo-4-chloro-benzonitrile

: 106-95-6
allyl bromide

: 1244549-41-4
4-chloro-2-allylbenzonitrile

Guidance literature:: 2-bromo-4-chloro-benzonitrile; With n-butyl magnesium bromide; n-butyllithium; In tetrahydrofuran; hexane; at -50 ℃; for 0.0833333h; Inert atmosphere;

allyl bromide; With copper(I) cyanide di(lithium chloride); In tetrahydrofuran; hexane; for 0.166667h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; hexane;
DOI:10.1021/ja1052126

Reference yield:

: 623-03-0
4-Cyanochlorobenzene

: 1244549-41-4
4-chloro-2-allylbenzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; N-Bromosuccinimide / 1,2-dichloro-ethane / Inert atmosphere; Schlenk technique

2: n-butyl magnesium bromide; lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Schlenk technique

With n-butyl magnesium bromide; N-Bromosuccinimide; lithium aluminium tetrahydride; palladium diacetate; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1002/anie.201405401