methyl(2'-(pyridin-2-yl)-[1,1'-biphenyl]-4-carboxylate)

Base Information

Chemical Name:methyl(2'-(pyridin-2-yl)-[1,1'-biphenyl]-4-carboxylate)
CAS No.:1245266-34-5
Molecular Formula:C₁₉H₁₅NO₂
Molecular Weight:289.334
Hs Code.:

Synonyms:methyl(2'-(pyridin-2-yl)-[1,1'-biphenyl]-4-carboxylate)

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Chemical Property of methyl(2'-(pyridin-2-yl)-[1,1'-biphenyl]-4-carboxylate)

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Technology Process of methyl(2'-(pyridin-2-yl)-[1,1'-biphenyl]-4-carboxylate)

There total 9 articles about methyl(2'-(pyridin-2-yl)-[1,1'-biphenyl]-4-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1008-89-5
2-phenylpyridine

: 1126-46-1
Methyl 4-chlorobenzoate

: 1245266-34-5
methyl(2'-(pyridin-2-yl)-[1,1'-biphenyl]-4-carboxylate)

Guidance literature:: With [dichloro(p-cymene)(triphenylphosphane)ruthenium(II)]; potassium carbonate; In water; at 80 ℃; for 4h; Inert atmosphere; Schlenk technique; Green chemistry;
DOI:10.1039/c2gc36222h

Reference yield: 67.0%

: 905966-40-7
methyl 4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzoate

: 89346-48-5
2-(2-fluorophenyl)pyridine

: 1245266-34-5
methyl(2'-(pyridin-2-yl)-[1,1'-biphenyl]-4-carboxylate)

Guidance literature:: With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; cesium fluoride; tricyclohexylphosphine; In toluene; at 20 - 100 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja207759e

Reference yield: 65.0%

: 1008-89-5
2-phenylpyridine

: 34040-64-7
p-methyloxycarbonylbenzyl chloride

: 1245266-34-5
methyl(2'-(pyridin-2-yl)-[1,1'-biphenyl]-4-carboxylate)

: 1209480-75-0
dimethyl 2'-(pyridin-2-yl)-[1,1':3',1''-terphenyl]-4,4''-dicarboxylate

Guidance literature:: With [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; water; potassium carbonate; levulinic acid; In isopropyl alcohol; at 80 ℃; for 4h; Inert atmosphere;
DOI:10.1002/ejic.201900218