2-<3-Benzodioxanylmethyl)-N-benzyl>aminopropyl>-3-oxo-5,5a,6,7-tetrahydro-2H,8H-pyridazino<4,5-b>pyrrolo<1,2-d><1,4>oxazine

Base Information

• Chemical Name: 2-<3-Benzodioxanylmethyl)-N-benzyl>aminopropyl>-3-oxo-5,5a,6,7-tetrahydro-2H,8H-pyridazino<4,5-b>pyrrolo<1,2-d><1,4>oxazine
• CAS No.: 134332-56-2
• Molecular Formula: C₂₈H₃₂N₄O₄
• Molecular Weight: 488.586

Synonyms:2-<3-Benzodioxanylmethyl)-N-benzyl>aminopropyl>-3-oxo-5,5a,6,7-tetrahydro-2H,8H-pyridazino<4,5-b>pyrrolo<1,2-d><1,4>oxazine

Chemical Property of 2-<3-Benzodioxanylmethyl)-N-benzyl>aminopropyl>-3-oxo-5,5a,6,7-tetrahydro-2H,8H-pyridazino<4,5-b>pyrrolo<1,2-d><1,4>oxazine

Chemical Property:

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Technology Process of 2-<3-Benzodioxanylmethyl)-N-benzyl>aminopropyl>-3-oxo-5,5a,6,7-tetrahydro-2H,8H-pyridazino<4,5-b>pyrrolo<1,2-d><1,4>oxazine

There total 4 articles about 2-<3-Benzodioxanylmethyl)-N-benzyl>aminopropyl>-3-oxo-5,5a,6,7-tetrahydro-2H,8H-pyridazino<4,5-b>pyrrolo<1,2-d><1,4>oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-<3-Benzodioxanylmethyl)-N-benzyl>aminopropyl>-4-chloro-5-(2-hydroxymethyl-1-pyrrolidinyl)-3(2H)-pyridazinone (134330-80-6) → 2-<3-Benzodioxanylmethyl)-N-benzyl>aminopropyl>-3-oxo-5,5a,6,7-tetrahydro-2H,8H-pyridazino<4,5-b>pyrrolo<1,2-d><1,4>oxazine (134332-56-2)

Guidance literature:

With sodium butanolate; In butan-1-ol; for 5h; Heating;

Reference yield:

(S)-4-Chloro-5-(2-hydroxymethyl-1-pyrrolidinyl)-3(2H)-pyridazinone (134330-76-0) → 2-<3-Benzodioxanylmethyl)-N-benzyl>aminopropyl>-3-oxo-5,5a,6,7-tetrahydro-2H,8H-pyridazino<4,5-b>pyrrolo<1,2-d><1,4>oxazine (134332-56-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) NaOEt, 2) tetrabutylammonium bromide / 1) ethanol, rt, 10 min, 2) toluene, 7 h, reflux

2: 93 percent / sodium butylate / butan-1-ol / 5 h / Heating

With tetrabutylammomium bromide; sodium ethanolate; sodium butanolate; In butan-1-ol;

Reference yield:

3-benzodioxanylmethyl)-N-benzyl)>aminopropylchloride (134330-85-1) → 2-<3-Benzodioxanylmethyl)-N-benzyl>aminopropyl>-3-oxo-5,5a,6,7-tetrahydro-2H,8H-pyridazino<4,5-b>pyrrolo<1,2-d><1,4>oxazine (134332-56-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) NaOEt, 2) tetrabutylammonium bromide / 1) ethanol, rt, 10 min, 2) toluene, 7 h, reflux

2: 93 percent / sodium butylate / butan-1-ol / 5 h / Heating

With tetrabutylammomium bromide; sodium ethanolate; sodium butanolate; In butan-1-ol;

upstream raw materials:

2-<3-Benzodioxanylmethyl)-N-benzyl>aminopropyl>-4-chloro-5-(2-hydroxymethyl-1-pyrrolidinyl)-3(2H)-pyridazinone

(S)-4-Chloro-5-(2-hydroxymethyl-1-pyrrolidinyl)-3(2H)-pyridazinone

3-benzodioxanylmethyl)-N-benzyl)>aminopropylchloride

(S)-1-Pyrrolidin-2-yl-methanol

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