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Technology Process of HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br(1+)*ClO4(1-)=[HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br]ClO4

HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br(1+)*ClO4(1-)=[HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br]ClO4

Base Information
  • Chemical Name:HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br(1+)*ClO4(1-)=[HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br]ClO4
  • CAS No.:256460-74-9
  • Molecular Formula:C14H21BrCoN6O4*ClO4
  • Molecular Weight:575.706
  • Hs Code.:
HONC(CH<sub>3</sub>)C(CH<sub>3</sub>)NOCH<sub>2</sub>ONC(CH<sub>3</sub>)C(CH<sub>3</sub>)NOCo(NC<sub>5</sub>H<sub>4</sub>NH<sub>2</sub>)Br<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=[HONC(CH<sub>3</sub>)C(CH<sub>3</sub>)NOCH<sub>2</sub>ONC(CH<sub>3</sub>)C(CH<sub>3</sub>)NOCo(NC<sub>5</sub>H<sub>4</sub>NH<sub>2</sub>)Br]ClO<sub>4</sub>

Synonyms:HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br(1+)*ClO4(1-)=[HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br]ClO4

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Chemical Property of HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br(1+)*ClO4(1-)=[HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br]ClO4
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Technology Process of HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br(1+)*ClO4(1-)=[HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br]ClO4

There total 1 articles about HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br(1+)*ClO4(1-)=[HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br]ClO4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.8%

2-aminopyridine
504-29-0

2-aminopyridine

HONC(CH<sub>3</sub>)C(CH<sub>3</sub>)NOCH<sub>2</sub>ONC(CH<sub>3</sub>)C(CH<sub>3</sub>)NOCoBr<sub>2</sub>
115381-20-9

HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCoBr2

sodium perchlorate

sodium perchlorate

HONC(CH<sub>3</sub>)C(CH<sub>3</sub>)NOCH<sub>2</sub>ONC(CH<sub>3</sub>)C(CH<sub>3</sub>)NOCo(NC<sub>5</sub>H<sub>4</sub>NH<sub>2</sub>)Br<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=[HONC(CH<sub>3</sub>)C(CH<sub>3</sub>)NOCH<sub>2</sub>ONC(CH<sub>3</sub>)C(CH<sub>3</sub>)NOCo(NC<sub>5</sub>H<sub>4</sub>NH<sub>2</sub>)Br]ClO<sub>4</sub>
256460-74-9

HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br(1+)*ClO4(1-)=[HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCo(NC5H4NH2)Br]ClO4

sodium bromide
7647-15-6

sodium bromide

Guidance literature:
In methanol; water; addn. of satd. aq. soln. of NaClO4 to hot suspn. of Co complex in MeOH, addn. of stoichiom. amt. of substituted pyridine in MeOH (stirring), refluxing (water bath, 4 h), pptn. on volume reduction and standing (35°, 2 h); filtration, washing (cold water, MeOH, Et2O), drying (vac.); elem. anal.;
DOI:10.1080/00945719909351731
upstream raw materials:

2-aminopyridine

HONC(CH3)C(CH3)NOCH2ONC(CH3)C(CH3)NOCoBr2

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