Technology Process of C30H46O6
There total 1 articles about C30H46O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium osmate(VI) dihydrate; potassium hexacyanoferrate (III); methanesulfonamide; C65H83N6O4(1+)*I(1-); potassium carbonate;
In
water; tert-butyl alcohol;
at 0 ℃;
for 19h;
regioselective reaction;
Inert atmosphere;
DOI:10.1021/ol200099n
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 0 - 20 ℃;
for 10h;
Inert atmosphere;
DOI:10.1021/ol200099n
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / dichloromethane / 10 h / 0 - 20 °C / Inert atmosphere
2.1: potassium carbonate / methanol; dichloromethane / Inert atmosphere
3.1: lithium hydroxide / methanol; water / 0.75 h / 65 °C / Inert atmosphere
3.2: 20 °C / Inert atmosphere
4.1: tetrabutylammomium bromide; magnesium bromide ethyl etherate / dichloromethane / 15 h / -78 - -40 °C / Inert atmosphere
With
pyridine; tetrabutylammomium bromide; potassium carbonate; magnesium bromide ethyl etherate; lithium hydroxide;
In
methanol; dichloromethane; water;
DOI:10.1021/ol200099n