1-(4-phenyl-1,2,3-triazol-1-yl)-1,2-dideoxy-2-amino-4,6-O-benzylidene-β-D-glucopyranose

Base Information

Chemical Name:1-(4-phenyl-1,2,3-triazol-1-yl)-1,2-dideoxy-2-amino-4,6-O-benzylidene-β-D-glucopyranose
CAS No.:1354639-06-7
Molecular Formula:C₂₁H₂₂N₄O₄
Molecular Weight:394.43
Hs Code.:

Synonyms:1-(4-phenyl-1,2,3-triazol-1-yl)-1,2-dideoxy-2-amino-4,6-O-benzylidene-β-D-glucopyranose

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Chemical Property of 1-(4-phenyl-1,2,3-triazol-1-yl)-1,2-dideoxy-2-amino-4,6-O-benzylidene-β-D-glucopyranose

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Technology Process of 1-(4-phenyl-1,2,3-triazol-1-yl)-1,2-dideoxy-2-amino-4,6-O-benzylidene-β-D-glucopyranose

There total 5 articles about 1-(4-phenyl-1,2,3-triazol-1-yl)-1,2-dideoxy-2-amino-4,6-O-benzylidene-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1354639-00-1
1-azido-4,6-O-benzylidene-1,2-dideoxy-2-amino-β-D-glucopyranose

: 536-74-3
phenylacetylene

: 1354639-06-7
1-(4-phenyl-1,2,3-triazol-1-yl)-1,2-dideoxy-2-amino-4,6-O-benzylidene-β-D-glucopyranose

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; In dichloromethane; water; for 8h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.11.043

Reference yield:

: 1354639-03-4
1-azido-3,4,6-tri-O-acetyl-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose

: 1354639-06-7
1-(4-phenyl-1,2,3-triazol-1-yl)-1,2-dideoxy-2-amino-4,6-O-benzylidene-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride; water / acetone / 70 °C / Inert atmosphere

2: camphor-10-sulfonic acid / acetonitrile / 2 h / Inert atmosphere; Reflux

3: ethylenediamine / Inert atmosphere; Microwave irradiation

4: copper(II) sulfate; sodium L-ascorbate / dichloromethane; water / 8 h / Inert atmosphere

With hydrogenchloride; camphor-10-sulfonic acid; water; copper(II) sulfate; sodium L-ascorbate; ethylenediamine; In dichloromethane; water; acetone; acetonitrile; 4: Huisgen cycloaddition;
DOI:10.1016/j.tetlet.2011.11.043

Reference yield:

: 1354639-05-6
1-azido-4,6-O-benzylidene-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose

: 1354639-06-7
1-(4-phenyl-1,2,3-triazol-1-yl)-1,2-dideoxy-2-amino-4,6-O-benzylidene-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: ethylenediamine / Inert atmosphere; Microwave irradiation

2: copper(II) sulfate; sodium L-ascorbate / dichloromethane; water / 8 h / Inert atmosphere

With copper(II) sulfate; sodium L-ascorbate; ethylenediamine; In dichloromethane; water; 2: Huisgen cycloaddition;
DOI:10.1016/j.tetlet.2011.11.043