1-azido-4,6-O-benzylidene-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose

Base Information

Chemical Name:1-azido-4,6-O-benzylidene-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose
CAS No.:1354639-05-6
Molecular Formula:C₂₁H₁₄Cl₄N₄O₆
Molecular Weight:560.177
Hs Code.:

Synonyms:1-azido-4,6-O-benzylidene-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose

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Chemical Property of 1-azido-4,6-O-benzylidene-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose

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Technology Process of 1-azido-4,6-O-benzylidene-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose

There total 3 articles about 1-azido-4,6-O-benzylidene-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 1354639-04-5
1-azido-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose

: 1354639-05-6
1-azido-4,6-O-benzylidene-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose

Guidance literature:: With camphor-10-sulfonic acid; In acetonitrile; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2011.11.043

Reference yield:

: 183388-13-8
1,3,4,6-tetra-O-acetyl-2-deoxy-2-tetrachlorophthaloylamino-α-D-glucopyranose

: 1354639-05-6
1-azido-4,6-O-benzylidene-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: tin(IV) chloride / dichloromethane / 7 h / Inert atmosphere

2: hydrogenchloride; water / acetone / 70 °C / Inert atmosphere

3: camphor-10-sulfonic acid / acetonitrile / 2 h / Inert atmosphere; Reflux

With hydrogenchloride; camphor-10-sulfonic acid; water; tin(IV) chloride; In dichloromethane; acetone; acetonitrile;
DOI:10.1016/j.tetlet.2011.11.043

Reference yield:

: 1354639-03-4
1-azido-3,4,6-tri-O-acetyl-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose

: 1354639-05-6
1-azido-4,6-O-benzylidene-1,2-dideoxy-2-(tetrachlorophthalimido)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / acetone / 70 °C / Inert atmosphere

2: camphor-10-sulfonic acid / acetonitrile / 2 h / Inert atmosphere; Reflux

With hydrogenchloride; camphor-10-sulfonic acid; water; In acetone; acetonitrile;
DOI:10.1016/j.tetlet.2011.11.043