HN(CH₂CH₂N=PPh₃)2

Base Information

Chemical Name:HN(CH₂CH₂N=PPh₃)2
CAS No.:1307274-00-5
Molecular Formula:C₄₀H₃₉N₃P₂
Molecular Weight:623.717
Hs Code.:

HN(CH<sub>2</sub>CH<sub>2</sub>N=PPh<sub>3</sub>)2

Synonyms:HN(CH₂CH₂N=PPh₃)2

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Chemical Property of HN(CH₂CH₂N=PPh₃)2

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Technology Process of HN(CH₂CH₂N=PPh₃)2

There total 1 articles about HN(CH₂CH₂N=PPh₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 111-40-0,98824-35-2
3-azapentane-1,5-diamine

: 1034-39-5
dibromotriphenylphosphorane

: 1307274-00-5
HN(CH₂CH₂N=PPh₃)2

Guidance literature:: 3-azapentane-1,5-diamine; dibromotriphenylphosphorane; With triethylamine; In dichloromethane; at 0 - 25 ℃; for 1h; Inert atmosphere;

With potassium hexamethylsilazane; In tetrahydrofuran; at 0 - 25 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c1dt10131e

Reference yield: 84.0%

: 1295-35-8
bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

: 108-86-1,52753-63-6
bromobenzene

: 1307274-00-5
HN(CH₂CH₂N=PPh₃)2

: 1310343-62-4
[HN(CH₂CH₂N=PPh₃)2Ni-C₆H₅][Br]

Guidance literature:: In tetrahydrofuran; (N2) ligand was added to Ni complex and bromobenzene in THF, stirred for1 h; solvent was decanted, ppt. was washed with ether and dried in vacuo, dissolved in CH2Cl2, filtered through Celite, evapd. in vacuo, triturated with ether and dried in vacuo; elem. anal.;
DOI:10.1039/c1dt10341e