4-(4'-hydroxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoic acid

Base Information

Chemical Name:4-(4'-hydroxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoic acid
CAS No.:157067-62-4
Molecular Formula:C₃₁H₄₄O₇
Molecular Weight:528.686
Hs Code.:

Synonyms:4-(4'-hydroxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoic acid

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Chemical Property of 4-(4'-hydroxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoic acid

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Technology Process of 4-(4'-hydroxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoic acid

There total 6 articles about 4-(4'-hydroxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 157067-58-8
benzyl 4-(4'-benzyloxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoate

: 157067-62-4
4-(4'-hydroxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 24h;

Reference yield:

: 61621-51-0
ethyl 2,4-dihydroxy-6-nonylbenzoate

: 157067-62-4
4-(4'-hydroxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / K₂CO₃ / acetone / 36 h / Heating

2: 81 percent / K₂CO₃ / dimethylformamide / 1.) 20 deg C, 24 h, 2.) 40 deg C, 4 h

3: 61 percent / KOH / dimethylsulfoxide; H₂O / 6.5 h / 90 °C

4: 97 percent / (CF₃CO)2O / toluene / 21 h / Ambient temperature

5: 80 percent / H₂ / 10percent Pd/C / ethyl acetate / 24 h

With potassium hydroxide; hydrogen; potassium carbonate; trifluoroacetic anhydride; palladium on activated charcoal; In water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 94693-37-5
benzyl 2-heptyl-4,6-dihydroxybenzoate

: 157067-62-4
4-(4'-hydroxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / (CF₃CO)2O / toluene / 21 h / Ambient temperature

2: 80 percent / H₂ / 10percent Pd/C / ethyl acetate / 24 h

With hydrogen; trifluoroacetic anhydride; palladium on activated charcoal; In ethyl acetate; toluene;