benzyl 4-(4'-benzyloxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoate

Base Information

Chemical Name:benzyl 4-(4'-benzyloxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoate
CAS No.:157067-58-8
Molecular Formula:C₄₅H₅₆O₇
Molecular Weight:708.935
Hs Code.:

Synonyms:benzyl 4-(4'-benzyloxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoate

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Chemical Property of benzyl 4-(4'-benzyloxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoate

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Technology Process of benzyl 4-(4'-benzyloxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoate

There total 5 articles about benzyl 4-(4'-benzyloxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 94693-37-5
benzyl 2-heptyl-4,6-dihydroxybenzoate

: 157067-53-3
4-benzyloxy-2-methoxy-6-nonylbenzoic acid

: 157067-58-8
benzyl 4-(4'-benzyloxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoate

Guidance literature:: With trifluoroacetic anhydride; In toluene; for 21h; Ambient temperature;

Reference yield:

: 61621-51-0
ethyl 2,4-dihydroxy-6-nonylbenzoate

: 157067-58-8
benzyl 4-(4'-benzyloxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / K₂CO₃ / acetone / 36 h / Heating

2: 81 percent / K₂CO₃ / dimethylformamide / 1.) 20 deg C, 24 h, 2.) 40 deg C, 4 h

3: 61 percent / KOH / dimethylsulfoxide; H₂O / 6.5 h / 90 °C

4: 97 percent / (CF₃CO)2O / toluene / 21 h / Ambient temperature

With potassium hydroxide; potassium carbonate; trifluoroacetic anhydride; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 100-39-0
benzyl bromide

: 157067-58-8
benzyl 4-(4'-benzyloxy-2'-methoxy-6'-nonylbenzoyloxy)-6-heptyl-2-hydroxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / K₂CO₃ / acetone / 36 h / Heating

2: 81 percent / K₂CO₃ / dimethylformamide / 1.) 20 deg C, 24 h, 2.) 40 deg C, 4 h

3: 61 percent / KOH / dimethylsulfoxide; H₂O / 6.5 h / 90 °C

4: 97 percent / (CF₃CO)2O / toluene / 21 h / Ambient temperature

With potassium hydroxide; potassium carbonate; trifluoroacetic anhydride; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene;