1-(2-acetamido-2-deoxy-3,4-O-isopropylidene-6-[tert-butyl(diphenyl)silyl]-α-D-galactopyranosyl)prop-2-ene

Base Information

Chemical Name:1-(2-acetamido-2-deoxy-3,4-O-isopropylidene-6-[tert-butyl(diphenyl)silyl]-α-D-galactopyranosyl)prop-2-ene
CAS No.:868527-80-4
Molecular Formula:C₃₀H₄₁NO₅Si
Molecular Weight:523.745
Hs Code.:

Synonyms:1-(2-acetamido-2-deoxy-3,4-O-isopropylidene-6-[tert-butyl(diphenyl)silyl]-α-D-galactopyranosyl)prop-2-ene

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Chemical Property of 1-(2-acetamido-2-deoxy-3,4-O-isopropylidene-6-[tert-butyl(diphenyl)silyl]-α-D-galactopyranosyl)prop-2-ene

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Technology Process of 1-(2-acetamido-2-deoxy-3,4-O-isopropylidene-6-[tert-butyl(diphenyl)silyl]-α-D-galactopyranosyl)prop-2-ene

There total 3 articles about 1-(2-acetamido-2-deoxy-3,4-O-isopropylidene-6-[tert-butyl(diphenyl)silyl]-α-D-galactopyranosyl)prop-2-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 868527-79-1
1-(2-acetamido-2-deoxy-6-[tert-butyl(diphenyl)silyl]-α-D-galactopyranosyl)prop-2-ene

: 77-76-9
2,2-dimethoxy-propane

: 868527-80-4
1-(2-acetamido-2-deoxy-3,4-O-isopropylidene-6-[tert-butyl(diphenyl)silyl]-α-D-galactopyranosyl)prop-2-ene

Guidance literature:: With Amberlite IR-120 (H⁺); In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1021/jo050691n

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 868527-80-4
1-(2-acetamido-2-deoxy-3,4-O-isopropylidene-6-[tert-butyl(diphenyl)silyl]-α-D-galactopyranosyl)prop-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / imidazole / dimethylformamide / 5 h / 20 °C

2: 100 percent / Amberlite IR-120 (H⁺) / dimethylformamide / 12 h / 20 °C

With 1H-imidazole; Amberlite IR-120 (H⁺); In N,N-dimethyl-formamide;
DOI:10.1021/jo050691n

Reference yield:

: 271246-14-1
1-(2'-acetamido-2'-deoxy-α-D-galactopyranosyl)-2-propene

: 868527-80-4
1-(2-acetamido-2-deoxy-3,4-O-isopropylidene-6-[tert-butyl(diphenyl)silyl]-α-D-galactopyranosyl)prop-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / imidazole / dimethylformamide / 5 h / 20 °C

2: 100 percent / Amberlite IR-120 (H⁺) / dimethylformamide / 12 h / 20 °C

With 1H-imidazole; Amberlite IR-120 (H⁺); In N,N-dimethyl-formamide;
DOI:10.1021/jo050691n