(Z)-4-phenyl-3-pentenoic acid phenyl amide

Base Information

Chemical Name:(Z)-4-phenyl-3-pentenoic acid phenyl amide
CAS No.:1252016-87-7
Molecular Formula:C₁₇H₁₇NO
Molecular Weight:251.328
Hs Code.:

Synonyms:(Z)-4-phenyl-3-pentenoic acid phenyl amide

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Chemical Property of (Z)-4-phenyl-3-pentenoic acid phenyl amide

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Technology Process of (Z)-4-phenyl-3-pentenoic acid phenyl amide

There total 2 articles about (Z)-4-phenyl-3-pentenoic acid phenyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 119271-86-2
(Z)-4-phenylpent-3-enoic acid

: 62-53-3
aniline

: 1252016-87-7
(Z)-4-phenyl-3-pentenoic acid phenyl amide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol101932q

Reference yield:

: 2288-18-8
2-phenyl-1,3-butadiene

: 201230-82-2
carbon monoxide

: 62-53-3
aniline

: 1252016-87-7
(Z)-4-phenyl-3-pentenoic acid phenyl amide

: (E)-N,4-diphenylpent-3-enamide

Guidance literature:: With palladium(II) trifluoroacetate; 1,2-bis[di(t-butyl)phosphinomethyl]benzene; In toluene; at 60 ℃; for 20h; under 67506.8 Torr; Overall yield = 74 %; regioselective reaction; Autoclave;
DOI:10.1021/ja507530f

Reference yield: 75.0%

: 1252016-87-7
(Z)-4-phenyl-3-pentenoic acid phenyl amide

: 1252016-88-8
(3R,4R)-3-hydroxy-4-phenylpentanamide

Guidance literature:: (Z)-4-phenyl-3-pentenoic acid phenyl amide; With bis(norbornadiene)rhodium(l)tetrafluoroborate; (4-tert-butylphenyl-TADDOL)POPh; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In tetrahydrofuran; at 0 - 40 ℃; for 25h; Inert atmosphere;

With water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 2h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol101932q