benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

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Chemical Name:benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside
CAS No.:912941-33-4
Molecular Formula:C₆₄H₈₉NO₁₁
Molecular Weight:1048.41
Hs Code.:

benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

Synonyms:benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

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Chemical Property of benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

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Technology Process of benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

There total 6 articles about benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 912941-32-3
formylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

: 912941-33-4
benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 20 °C

2: 885.6 mg / CH₂Cl₂; diethyl ether / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmc.2006.05.051

Reference yield:

: 912941-31-2
allyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

: 912941-33-4
benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 4-methylmorpholine-N-oxide; OsO₄ / tetrahydrofuran; 2-methyl-propan-2-ol; H₂O / 8 h / 20 °C

2: 109.2 mg / Pb(OAc)4 / benzene / 1 h / 20 °C

3: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 20 °C

4: 885.6 mg / CH₂Cl₂; diethyl ether / 20 °C

With lead(IV) acetate; sodium chlorite; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; 4-methylmorpholine N-oxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol; benzene;
DOI:10.1016/j.bmc.2006.05.051

Reference yield:

: (R)-3-Benzyloxy-tetradecanoic acid (2R,4aR,6S,7R,8R,8aS)-7-((R)-3-benzyloxy-tetradecanoylamino)-6-(2,3-dihydroxy-propoxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yl ester

: 912941-33-4
benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 109.2 mg / Pb(OAc)4 / benzene / 1 h / 20 °C

2: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 20 °C

3: 885.6 mg / CH₂Cl₂; diethyl ether / 20 °C

With lead(IV) acetate; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In diethyl ether; dichloromethane; water; tert-butyl alcohol; benzene;
DOI:10.1016/j.bmc.2006.05.051