benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-6-O-(N-(9-fluorenylmethoxycarbonyl)-O-tert-butyl-D-seryl)-α-D-glucopyranoside

Base Information

Chemical Name:benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-6-O-(N-(9-fluorenylmethoxycarbonyl)-O-tert-butyl-D-seryl)-α-D-glucopyranoside
CAS No.:912941-35-6
Molecular Formula:C₇₉H₁₀₈N₂O₁₅
Molecular Weight:1325.73
Hs Code.:

benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-6-O-(N-(9-fluorenylmethoxycarbonyl)-O-tert-butyl-D-seryl)-α-D-glucopyranoside

Synonyms:benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-6-O-(N-(9-fluorenylmethoxycarbonyl)-O-tert-butyl-D-seryl)-α-D-glucopyranoside

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Chemical Property of benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-6-O-(N-(9-fluorenylmethoxycarbonyl)-O-tert-butyl-D-seryl)-α-D-glucopyranoside

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Technology Process of benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-6-O-(N-(9-fluorenylmethoxycarbonyl)-O-tert-butyl-D-seryl)-α-D-glucopyranoside

There total 8 articles about benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-6-O-(N-(9-fluorenylmethoxycarbonyl)-O-tert-butyl-D-seryl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 912941-34-5
benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-2-α-D-glucopyranoside

: 71989-33-8,128107-47-1
Nα-(9-fluorenylmethoxycarbonyl)-D-serine-tert-butyl ether

: 912941-35-6
benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-6-O-(N-(9-fluorenylmethoxycarbonyl)-O-tert-butyl-D-seryl)-α-D-glucopyranoside

Guidance literature:: With 1-methyl-1H-imidazole; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In tetrahydrofuran; at 20 ℃; for 13h;
DOI:10.1016/j.bmc.2006.05.051

Reference yield:

: 912941-32-3
formylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

: 912941-35-6
benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-6-O-(N-(9-fluorenylmethoxycarbonyl)-O-tert-butyl-D-seryl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 20 °C

2: 885.6 mg / CH₂Cl₂; diethyl ether / 20 °C

3: 90 percent / trifluoroacetic acid / CH₂Cl₂; H₂O / 0.67 h / 20 °C

4: 85 percent / 1-(2,4,6-trimethylphenylsulfonyl)-3-nitro-1,2,4-triazole; N-methylimidazole / tetrahydrofuran / 13 h / 20 °C

With 1-methyl-1H-imidazole; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmc.2006.05.051

Reference yield:

: 912941-33-4
benzyloxycarbonylmethyl 4,6-O-benzylidene-3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-α-D-glucopyranoside

: 912941-35-6
benzyloxycarbonylmethyl 3-O-((R)-3-benzyloxytetradecanoyl)-2-((R)-3-benzyloxytetradecanoylamino)-2-deoxy-6-O-(N-(9-fluorenylmethoxycarbonyl)-O-tert-butyl-D-seryl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / trifluoroacetic acid / CH₂Cl₂; H₂O / 0.67 h / 20 °C

2: 85 percent / 1-(2,4,6-trimethylphenylsulfonyl)-3-nitro-1,2,4-triazole; N-methylimidazole / tetrahydrofuran / 13 h / 20 °C

With 1-methyl-1H-imidazole; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.bmc.2006.05.051