3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoic acid

Base Information

Chemical Name:3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoic acid
CAS No.:1610861-75-0
Molecular Formula:C₂₀H₃₁N₃O₇S
Molecular Weight:457.548
Hs Code.:

Synonyms:3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoic acid

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Chemical Property of 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoic acid

Chemical Property:

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Technology Process of 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoic acid

There total 6 articles about 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610861-77-2
benzyl 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoate

: 1610861-75-0
3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; water; for 5h; under 1551.49 Torr;

Reference yield:

: 89-41-8
4-methoxy-3-nitrobenzoic acid

: 1610861-75-0
3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 8 h / 20 °C

2.1: ammonium chloride; iron / water; ethanol / 2 h / 80 °C

3.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: ethanol / 20 °C

5.1: dmap / dichloromethane / 28 h / 20 °C

6.1: palladium 10% on activated carbon; hydrogen / methanol; water / 5 h / 1551.49 Torr

With pyridine; dmap; palladium 10% on activated carbon; hydrogen; iron; ammonium chloride; caesium carbonate; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1610861-79-4
benzyl 4-methoxy-3-(2-(4-methylpiperazin-1-yl)ethylsulfonamido)benzoate

: 1610861-75-0
3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: dmap / dichloromethane / 28 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol; water / 5 h / 1551.49 Torr

With dmap; palladium 10% on activated carbon; hydrogen; In methanol; dichloromethane; water;