benzyl 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoate

Base Information

Chemical Name:benzyl 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoate
CAS No.:1610861-77-2
Molecular Formula:C₂₇H₃₇N₃O₇S
Molecular Weight:547.673
Hs Code.:

Synonyms:benzyl 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoate

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Chemical Property of benzyl 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoate

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Technology Process of benzyl 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoate

There total 6 articles about benzyl 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1610861-79-4
benzyl 4-methoxy-3-(2-(4-methylpiperazin-1-yl)ethylsulfonamido)benzoate

: 1610861-77-2
benzyl 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoate

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 28h;

Reference yield:

: 100-39-0
benzyl bromide

: 1610861-77-2
benzyl 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 8 h / 20 °C

2.1: ammonium chloride; iron / water; ethanol / 2 h / 80 °C

3.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: ethanol / 20 °C

5.1: dmap / dichloromethane / 28 h / 20 °C

With pyridine; dmap; iron; ammonium chloride; caesium carbonate; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 89-41-8
4-methoxy-3-nitrobenzoic acid

: 1610861-77-2
benzyl 3-(N-(tert-butoxycarbonyl)-2-(4-methylpiperazin-1-yl)ethylsulfonamido)-4-methoxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 8 h / 20 °C

2.1: ammonium chloride; iron / water; ethanol / 2 h / 80 °C

3.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

4.1: ethanol / 20 °C

5.1: dmap / dichloromethane / 28 h / 20 °C

With pyridine; dmap; iron; ammonium chloride; caesium carbonate; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;